3-Hydroxy-4-methoxybenzyl bromide

Base Information

Chemical Name:3-Hydroxy-4-methoxybenzyl bromide
CAS No.:111394-51-5
Molecular Formula:C8H9BrO2
Molecular Weight:217.062
Hs Code.:
DSSTox Substance ID:DTXSID60552939
Nikkaji Number:J2.793.733K
Wikidata:Q82433369
Mol file:111394-51-5.mol

Synonyms:111394-51-5;5-(BROMOMETHYL)-2-METHOXYPHENOL;3-hydroxy-4-methoxybenzyl bromide;SCHEMBL6401380;DTXSID60552939;HJDXWELICJVYDY-UHFFFAOYSA-N;EN300-1910562

Suppliers and Price of 3-Hydroxy-4-methoxybenzyl bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-Hydroxy-4-methoxybenzyl bromide

Chemical Property:

XLogP3:2.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:215.97859
Heavy Atom Count:11
Complexity:119

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)CBr)O

Technology Process of 3-Hydroxy-4-methoxybenzyl bromide

There total 2 articles about 3-Hydroxy-4-methoxybenzyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 4383-06-6
3-hydroxy-4-methoxybenzyl alcohol

: 111394-51-5
3-hydroxy-4-methoxybenzyl bromide

Guidance literature:: With phosphorus tribromide; In diethyl ether; at 0 ℃; for 0.5h; Inert atmosphere;
DOI:10.1016/j.bmc.2016.09.063

Reference yield:

: 621-59-0
isovanillin

: 111394-51-5
3-hydroxy-4-methoxybenzyl bromide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 2 h / 20 °C

2: phosphorus tribromide / diethyl ether / 0.5 h / 0 °C

With sodium tetrahydroborate; phosphorus tribromide; In methanol; diethyl ether;
DOI:10.1016/j.bmcl.2013.10.010

Reference yield: 92.0%

: 111394-51-5
3-hydroxy-4-methoxybenzyl bromide

: 621-59-0
isovanillin

Guidance literature:: With water; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; at 50 ℃; for 0.916667h; Ionic liquid; Inert atmosphere;
DOI:10.1080/00397910902840835