1,3-Dimesitylpropane

Base Information

Chemical Name:1,3-Dimesitylpropane
CAS No.:111514-28-4
Molecular Formula:C21H28
Molecular Weight:280.44700
Hs Code.:
DSSTox Substance ID:DTXSID40534839
Nikkaji Number:J174.668E
Wikidata:Q82408849
Mol file:111514-28-4.mol

Synonyms:1,3-dimesitylpropane;111514-28-4;DTXSID40534839;1,1'-(Propane-1,3-diyl)bis(2,4,6-trimethylbenzene)

Suppliers and Price of 1,3-Dimesitylpropane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,3-Dimesitylpropane

Chemical Property:

PSA：0.00000
LogP:5.71230
XLogP3:6.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:4
Exact Mass:280.219100893
Heavy Atom Count:21
Complexity:253

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)C)CCCC2=C(C=C(C=C2C)C)C)C

Technology Process of 1,3-Dimesitylpropane

There total 1 articles about 1,3-Dimesitylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1,3-dimesitylpropanon-1

: 111514-28-4
1,3-dimesitylpropane

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; 0.5 h, 2 h reflux;
DOI:10.1016/0022-328X(87)87133-4

Reference yield: 88.0%

: 37366-09-9
dichloro(benzene)ruthenium(II) dimer

: tetrafluoroboric acid

: 111514-28-4
1,3-dimesitylpropane

: RuC₆H₆C₂₁H₂₈⁽²⁺⁾*2BF₄^(1-)

Guidance literature:: In trifluoroacetic acid; mixt. of reagents in CF3COOH was refluxed for 2 h; after cooling mixt. was filtered, aq. HBF4 was added;; evapd., washed with ether, recrystd. from MeNO2-EtOH; elem. anal.;;
DOI:10.1016/0022-328X(87)87133-4

Reference yield: 88.0%

: 37366-09-9
dichloro(benzene)ruthenium(II) dimer

: tetrafluoroboric acid

: 75-52-5
nitromethane

: 111514-28-4
1,3-dimesitylpropane

: (C₆H₆)Ru((C₆H₂(CH₃)3)(CH₂)3(C₆H₂(CH₃)3))⁽²⁺⁾*2BF₄^(1-)*CH₃NO₂={(C₆H₆)Ru((C₆H₂(CH₃)3)(CH₂)3(C₆H₂(CH₃)3))}(BF₄)2*CH₃NO₂

Guidance literature:: In trifluoroacetic acid; boiling a mixt. of the complex and 1,3-dimesitylpropane (2 h, large excess of ligand, protection from atmospheric moisture) in CF3COOH until the orange color is vanishing, cooling, filtering, concg., filtering, evapg. the filtrate, adding 48% aq. HBF4; evapg. (vac.) to dryness, recrystn. (MeNO2/EtOH); elem. anal.;