1-[2-(Benzyloxy)ethoxy]-4-bromobenzene

Base Information

Chemical Name:1-[2-(Benzyloxy)ethoxy]-4-bromobenzene
CAS No.:111660-11-8
Molecular Formula:C15H15BrO2
Molecular Weight:307.187
Hs Code.:
DSSTox Substance ID:DTXSID30552224
Wikidata:Q82432323
Mol file:111660-11-8.mol

Synonyms:111660-11-8;1-[2-(BENZYLOXY)ETHOXY]-4-BROMOBENZENE;SCHEMBL3120643;DTXSID30552224;GTRFMRBPSUSTPA-UHFFFAOYSA-N;1-(2-benzyloxyethoxy)-4-bromobenzene;AKOS005974564;1-(2-benzyloxy-ethoxy)-4-bromobenzene;1-(2-Benzyloxy-ethoxy)-4-bromo-benzene

Suppliers and Price of 1-[2-(Benzyloxy)ethoxy]-4-bromobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 1-[2-(Benzyloxy)ethoxy]-4-bromobenzene

Chemical Property:

PSA：18.46000
LogP:4.04470
XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:306.02554
Heavy Atom Count:18
Complexity:209

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)COCCOC2=CC=C(C=C2)Br

Technology Process of 1-[2-(Benzyloxy)ethoxy]-4-bromobenzene

There total 2 articles about 1-[2-(Benzyloxy)ethoxy]-4-bromobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 111660-11-8
1-[2-(benzyloxy)ethoxy]-4-bromobenzene

Guidance literature:: 2-(4-bromophenoxy)ethanol; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.333333h;

benzyl bromide; In N,N-dimethyl-formamide; for 13h;

Reference yield:

: 106-41-2
4-bromo-phenol

: 1462-37-9
bromoethyl-2-benzyl ether

: 111660-11-8
1-[2-(benzyloxy)ethoxy]-4-bromobenzene

Guidance literature:: With potassium carbonate; In butanone; at 80 ℃;

Reference yield: 69.0%

: 111660-11-8
1-[2-(benzyloxy)ethoxy]-4-bromobenzene

: 916060-45-2
1,1'-bis(t-butoxycarbonyl)-4,4'-dibromo-6,6'-dimethyl-2,2'-bisbenzimidazole

: 1,1'-bis(t-butoxycarbonyl)-4,4'-bis{4-[2-(benzyloxy)ethoxy]phenyl}-6,6'-dimethyl-2,2'-bisbenzimidazole

Guidance literature:: 1-[2-(benzyloxy)ethoxy]-4-bromobenzene; With n-butyllithium; zinc(II) chloride; In tetrahydrofuran; hexane; at -78 - 0 ℃;

1,1'-bis(t-butoxycarbonyl)-4,4'-dibromo-6,6'-dimethyl-2,2'-bisbenzimidazole; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; at 60 ℃; for 6h;
DOI:10.1021/ol061244c