5-[(2-nitrophenyl)hydrazinylidene]-1,3-diazinane-2,4,6-trione

Base Information

• Chemical Name: 5-[(2-nitrophenyl)hydrazinylidene]-1,3-diazinane-2,4,6-trione
• CAS No.: 111709-57-0
• Molecular Formula: C10H7N5O5
• Molecular Weight: 277.196
• Mol file: 111709-57-0.mol

Synonyms:5,6-Dioxyuracil;2,4,5,6-Tetraoxypyrimidine;alloxane tetrahydrate;Alloxan tetrahydrate;

Chemical Property of 5-[(2-nitrophenyl)hydrazinylidene]-1,3-diazinane-2,4,6-trione

Chemical Property:

• PSA: 145.48000
• LogP: 0.98250

Purity/Quality:

99% ^*data from raw suppliers

5-[(2-nitrophenyl)hydrazono]-2,4,6(1H,3H,5H)-pyrimidinetrione ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-[(2-nitrophenyl)hydrazinylidene]-1,3-diazinane-2,4,6-trione

There total 2 articles about 5-[(2-nitrophenyl)hydrazinylidene]-1,3-diazinane-2,4,6-trione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

BARBITURIC ACID (67-52-7,944357-77-1) + 2-nitro-aniline (88-74-4) → pyrimidine-2(1H),4(3H),5,6-tetraone-5-(2-nitrophenyl)-hydrazone (111709-57-0)

Guidance literature:

With hydrogenchloride; sodium acetate; sodium nitrite; Yield given. Multistep reaction; 1) water, 5 min, 0 deg C 2) methanol, room temperature;

DOI:10.1039/P29870000469

Reference yield:

BARBITURIC ACID (67-52-7,944357-77-1) → pyrimidine-2(1H),4(3H),5,6-tetraone-5-(2-nitrophenyl)-hydrazone (111709-57-0)

Guidance literature:

With hydrogenchloride;

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + pyrimidine-2(1H),4(3H),5,6-tetraone-5-(2-nitrophenyl)-hydrazone (111709-57-0) → uramil (118-78-5)

Guidance literature:

upstream raw materials:

BARBITURIC ACID

2-nitro-aniline

Downstream raw materials:

uramil

Refernces

• 1、 Beaton, Haydn G.,Willey, Gerald R.,Drew, Michael G. B.. "Preparation and Hydrogen Bonding Studies of Phenylhydrazone Derivatives of Alloxan: Crystal and Molecular Structure of Pyrimidine-2(1H),4(3H),5,6-tetraone-5-(2-Nitrophenyl)hydrazone". . p. 469 - 472. Retrieved 2007/10/02.