SALICYLIDENE BENZHYDRAZIDE

Base Information

• Chemical Name: SALICYLIDENE BENZHYDRAZIDE
• CAS No.: 3232-37-9
• Molecular Formula: C14H12 N2 O2
• Molecular Weight: 240.26
• Hs Code.: 2928000090
• Mol file: 3232-37-9.mol

Synonyms:Benzoicacid, [(2-hydroxyphenyl)methylene]hydrazide (9CI); Benzoic acid,salicylidenehydrazide (6CI,7CI,8CI); Benzoic acid salicylalhydrazide; Benzoylsalicylal hydrazone; NSC 148180; Salicylaldehyde benzoylhydrazone; Salicylidenebenzoyl hydrazine; Salicylidenebenzohydrazide; o-Hydroxybenzaldehydebenzoylhydrazone

Chemical Property of SALICYLIDENE BENZHYDRAZIDE

Chemical Property:

• PSA: 61.69000
• Density: 1.172g/cm³
• LogP: 2.54700

Purity/Quality:

98%min ^*data from raw suppliers

Salicylidene benzoylhydrazone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of SALICYLIDENE BENZHYDRAZIDE

There total 8 articles about SALICYLIDENE BENZHYDRAZIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

salicylaldehyde (90-02-8) + benzoic acid hydrazide (613-94-5) → salicylaldehyde benzoylhydrazone (3232-37-9,71112-98-6)

Guidance literature:

In methanol; water; at 20 ℃;

DOI:10.1021/acs.orglett.6b03174

Reference yield: 96.0%

2-methyl-benzyl alcohol (89-95-2) + benzoic acid hydrazide (613-94-5) → salicylaldehyde benzoylhydrazone (3232-37-9,71112-98-6)

Guidance literature:

at 75 ℃; for 0.025h; microwave irradiation;

Reference yield:

(1-hydroxybenzo[d][1,2,3]diazaborinin-2(1 H)yl)(phenyl)methanone → salicylaldehyde benzoylhydrazone (3232-37-9,71112-98-6)

Guidance literature:

With dihydrogen peroxide; In N,N-dimethyl-formamide; at 25 ℃; for 0.5h; pH=7.4;

DOI:10.1002/anie.202109835

upstream raw materials:

salicylaldehyde

benzoic acid hydrazide

2-methyl-benzyl alcohol

benzoic acid

Downstream raw materials:

2-acetylbenzaldehyde