2-(2-Acetyloxyethoxy)terephthalic acid

Base Information

Chemical Name:2-(2-Acetyloxyethoxy)terephthalic acid
CAS No.:111822-81-2
Molecular Formula:C12H12O7
Molecular Weight:268.223
Hs Code.:
DSSTox Substance ID:DTXSID701220991
Mol file:111822-81-2.mol

Synonyms:111822-81-2;DTXSID701220991;2-[2-(Acetyloxy)ethoxy]-1,4-benzenedicarboxylic acid

Suppliers and Price of 2-(2-Acetyloxyethoxy)terephthalic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(2-Acetyloxyethoxy)terephthalic acid

Chemical Property:

XLogP3:0.7
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:268.05830272
Heavy Atom Count:19
Complexity:352

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=O)OCCOC1=C(C=CC(=C1)C(=O)O)C(=O)O

Technology Process of 2-(2-Acetyloxyethoxy)terephthalic acid

There total 3 articles about 2-(2-Acetyloxyethoxy)terephthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: 111822-80-1
2-(2'-hydroxyethoxy)terephthalic acid

: 5-Oxo-2,3-dihydro-5H-benzo[e][1,4]dioxepine-8-carboxylic acid

: 111822-81-2
2-(2'-acetoxyethoxy)terephthalic acid

Guidance literature:: With pyridine; In chloroform; for 2h; Heating;
DOI:10.1021/jo00237a044

Reference yield:

: 636-94-2
2-hydroxyterephthalic acid

: 111822-81-2
2-(2'-acetoxyethoxy)terephthalic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaOH / H₂O / 48 h / Ambient temperature

2: 92 percent / pyridine / CHCl₃ / 2 h / Heating

With pyridine; sodium hydroxide; In chloroform; water;
DOI:10.1021/jo00237a044

Reference yield:

: 586-35-6
2-bromo-1,4-benzenedicarboxylic acid

: 111822-81-2
2-(2'-acetoxyethoxy)terephthalic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / NaOH, NaOAc, Cu / H₂O / 72 h / Heating

2: 76 percent / NaOH / H₂O / 48 h / Ambient temperature

3: 92 percent / pyridine / CHCl₃ / 2 h / Heating

With pyridine; sodium hydroxide; sodium acetate; copper; In chloroform; water;
DOI:10.1021/jo00237a044