arthrobactin

Base Information

• Chemical Name: arthrobactin
• CAS No.: 39007-57-3
• Molecular Formula: C₂₀H₃₆N₄O₉
• Molecular Weight: 476.527
• Mol file: 39007-57-3.mol

Synonyms:Arthrobactin

Chemical Property of arthrobactin

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 203.79000
• Density: 1.3g/cm³
• LogP: 1.31130

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of arthrobactin

There total 12 articles about arthrobactin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Sodium; 3-[5-(acetyl-benzyloxy-amino)-pentylcarbamoyl]-2-{[5-(acetyl-benzyloxy-amino)-pentylcarbamoyl]-methyl}-2-hydroxy-propionate (83948-79-2) → Arthrobactin (39007-57-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; water; for 3h; under 760 Torr; Yield given; Ambient temperature;

DOI:10.1021/jo00149a005

Reference yield:

N-[5-(Acetyl-benzyloxy-amino)-pentyl]-2-{[5-(acetyl-benzyloxy-amino)-pentylcarbamoyl]-methyl}-2-hydroxy-succinamic acid → Arthrobactin (39007-57-3)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; water; for 3h; under 760 Torr;

DOI:10.1021/jo00079a007

Reference yield:

N-[5-(Acetyl-benzyloxy-amino)-pentyl]-2-{[5-(acetyl-benzyloxy-amino)-pentylcarbamoyl]-methyl}-2-hydroxy-succinamic acid tert-butyl ester (153492-05-8) → Arthrobactin (39007-57-3)

Guidance literature:

Multi-step reaction with 2 steps

1: TFA / CH₂Cl₂ / 0.5 h

2: H₂ / 10percent Pd/C / tetrahydrofuran; H₂O / 3 h / 760 Torr

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; water;

DOI:10.1021/jo00079a007

upstream raw materials:

Sodium; 3-[5-(acetyl-benzyloxy-amino)-pentylcarbamoyl]-2-{[5-(acetyl-benzyloxy-amino)-pentylcarbamoyl]-methyl}-2-hydroxy-propionate

N-[5-(Acetyl-benzyloxy-amino)-pentyl]-2-{[5-(acetyl-benzyloxy-amino)-pentylcarbamoyl]-methyl}-2-hydroxy-succinamic acid tert-butyl ester

5-hydroxypentylamine

5-oxo-1,3-dioxolan-4-ylidenedi(acetic acid)