4-Quinolinol, 2-methyl-, benzoate (ester)

Base Information

• Chemical Name: 4-Quinolinol, 2-methyl-, benzoate (ester)
• CAS No.: 111947-01-4
• Molecular Formula: C17H13NO2
• Molecular Weight: 263.296
• Mol file: 111947-01-4.mol

Synonyms:Benzoesaeure-(2-methyl-[4]chinolylester);benzoic acid-(2-methyl-[4]quinolyl ester);

Chemical Property of 4-Quinolinol, 2-methyl-, benzoate (ester)

Chemical Property:

• PSA: 39.19000
• LogP: 3.76240

Purity/Quality:

95+% ^*data from raw suppliers

2-Methylquinolin-4-ylbenzoate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-Quinolinol, 2-methyl-, benzoate (ester)

There total 3 articles about 4-Quinolinol, 2-methyl-, benzoate (ester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

4-hydroxy-2-methylquinoline (607-67-0) + benzoyl chloride (98-88-4) → 2-methylquinolin-4-yl benzoate (111947-01-4)

Guidance literature:

With 4-methyl-morpholine; In dichloromethane; at 10 - 25 ℃;

DOI:10.1002/adsc.201100141

Reference yield:

4-hydroxy-2-methylquinoline (607-67-0) + benzoic acid (65-85-0,8013-63-6) → 2-methylquinolin-4-yl benzoate (111947-01-4)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In tetrahydrofuran; at 25 ℃;

DOI:10.1039/c8ra04984j

Reference yield:

benzoyl chloride (98-88-4) → 2-methylquinolin-4-yl benzoate (111947-01-4)

Guidance literature:

With diethyl ether;

upstream raw materials:

benzoyl chloride

4-hydroxy-2-methylquinoline

benzoic acid

Downstream raw materials:

(4-hydroxy-2-methyl-quinolin-3-yl)-phenyl-methanone

4-(4-fluorophenyl)-2-methylquinoline

2-methyl-4-(o-tolyl)quinoline

2-(2-ethylquinolin-4-yl)benzaldehyde

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