n,n-Dimethylundec-10-enamide

Base Information

• Chemical Name: n,n-Dimethylundec-10-enamide
• CAS No.: 24928-46-9
• Molecular Formula: C13H25 N O
• Molecular Weight: 211.348
• NSC Number: 70032
• DSSTox Substance ID: DTXSID10947811
• Nikkaji Number: J264.002C
• Wikidata: Q82925631
• Mol file: 24928-46-9.mol

Synonyms:n,n-dimethylundec-10-enamide;24928-46-9;N,N-Dimethyl-10-undecenamide;NSC70032;SCHEMBL3112734;DTXSID10947811;NSC-70032

Chemical Property of n,n-Dimethylundec-10-enamide

Chemical Property:

• Vapor Pressure: 0.000663mmHg at 25°C
• Boiling Point: 308.8°Cat760mmHg
• Flash Point: 126.1°C
• Density: 0.871g/cm³
• XLogP3: 3.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 9
• Exact Mass: 211.193614421
• Heavy Atom Count: 15
• Complexity: 175

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CN(C)C(=O)CCCCCCCCC=C

Technology Process of n,n-Dimethylundec-10-enamide

There total 1 articles about n,n-Dimethylundec-10-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

S-ethyl 10-thioundecenoate + N,N-dimethyl-formamide (68-12-2,33513-42-7) → docosa-1,21-diene-11,12-dione (79186-36-0) + 10-undecenoic acid (112-38-9) + N,N-dimethylundec-10-enamide (24928-46-9) + Undec-10-enethioic acid (103199-96-8)

Guidance literature:

With lithium perchlorate; Electrochemical reaction;

DOI:10.1016/j.tet.2004.12.050

Reference yield: 36.0%

N,N-dimethylundec-10-enamide (24928-46-9) → 10-Undecen-1-ol (112-43-6)

Guidance literature:

With ethanol; sodium; In hexane; paraffin oil; at 0 ℃; for 0.0833333h; Inert atmosphere;

Reference yield:

N,N-dimethylundec-10-enamide (24928-46-9) → 10-Undecen-1-ol (112-43-6) + N,N-dimethyl-10-undecen-1-amine (34832-45-6)

Guidance literature:

With ethanol; sodium; In hexane; at 0 ℃; for 0.333333h; Overall yield = 83 %; Overall yield = 70.7 mg; chemoselective reaction; Inert atmosphere;

DOI:10.1021/acs.joc.8b00617

upstream raw materials:

N,N-dimethyl-formamide

Downstream raw materials:

10-Undecenal

10-Undecen-1-ol

N,N-dimethyl-10-undecen-1-amine