1,3-Bis(6,11-dihydrodibenzo(b,e)thiepin-11-yl)urea

Base Information

Chemical Name:1,3-Bis(6,11-dihydrodibenzo(b,e)thiepin-11-yl)urea
CAS No.:74797-32-3
Molecular Formula:C₂₉H₂₄N₂OS₂
Molecular Weight:480.654
Hs Code.:
DSSTox Substance ID:DTXSID50996323
Mol file:74797-32-3.mol

Synonyms:74797-32-3;BRN 4608089;1,3-Bis(6,11-dihydrodibenzo(b,e)thiepin-11-yl)urea;VUFB-12441;1,3-bis(6,11-dihydrobenzo[c][1]benzothiepin-11-yl)urea;Urea, N,N'-bis(6,11-dihydrodibenzo(b,e)thiepin-11-yl)-;Oprea1_017058;C29H24N2OS2;DTXSID50996323;JCNLVFDVRCTBMB-UHFFFAOYSA-N;C29-H24-N2-O-S2;AKOS005066047;LS-159048;AE-641/30116057;N,N'-di(6,11-dihydrodibenzo[b,e]thiepin-11-yl)urea;N,N'-Bis[(6,11-dihydrodibenzo[b,e]thiepin-11-yl)]carbamimidic acid

Suppliers and Price of 1,3-Bis(6,11-dihydrodibenzo(b,e)thiepin-11-yl)urea

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
1,3-BIS-(6,11-DIHYDRODIBENZO(B,E)THIEPIN-11-YL)UREA 95.00%
5MG
$ 500.29

Total 4 raw suppliers

Chemical Property of 1,3-Bis(6,11-dihydrodibenzo(b,e)thiepin-11-yl)urea

Chemical Property:

Vapor Pressure:2.57E-19mmHg at 25°C
Boiling Point:697.7°C at 760 mmHg
Flash Point:375.8°C
PSA：95.22000
Density:1.36g/cm³
LogP:7.67150
XLogP3:5.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:480.13300574
Heavy Atom Count:34
Complexity:648

Purity/Quality:

99% ^*data from raw suppliers

1,3-BIS-(6,11-DIHYDRODIBENZO(B,E)THIEPIN-11-YL)UREA 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C2C(C3=CC=CC=C3S1)NC(=O)NC4C5=CC=CC=C5CSC6=CC=CC=C46

Technology Process of 1,3-Bis(6,11-dihydrodibenzo(b,e)thiepin-11-yl)urea

There total 2 articles about 1,3-Bis(6,11-dihydrodibenzo(b,e)thiepin-11-yl)urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1745-46-6
6,11-dihydrodibenzo[b,e]thiepin-11-ol

: 74797-32-3
1,3-bis(6,11-dihydrodibenzothiepin-11-yl)urea

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / 4-toluenesulfonic acid / acetic acid / 1) 37 deg C, 6h; 2) room temp., overnight

2: 1) Na / 1) 2-diethylaminoethanol; 2) 8 h, 160-180 deg C

With sodium; toluene-4-sulfonic acid; In acetic acid;
DOI:10.1135/cccc19800517