[1,1'-Bicyclohexyl]-2,3'-dione, 6-(trimethylstannyl)-

Base Information

Chemical Name:[1,1'-Bicyclohexyl]-2,3'-dione, 6-(trimethylstannyl)-
CAS No.:112080-44-1
Molecular Formula:C₁₅H₂₆O₂Sn
Molecular Weight:357.08
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,1'-Bicyclohexyl]-2,3'-dione, 6-(trimethylstannyl)-

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Technology Process of [1,1'-Bicyclohexyl]-2,3'-dione, 6-(trimethylstannyl)-

There total 1 articles about [1,1'-Bicyclohexyl]-2,3'-dione, 6-(trimethylstannyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 930-68-7
cyclohexenone

: 89041-25-8
(trimethylstannyl)copper(I)-dimethyl sulfide

: 112080-44-1
2-(3-ketocyclohexyl)-3-trimethylstannylcyclohexanone

: 63831-50-5,149655-21-0
3-(trimethylstannyl)cyclohexanone

Guidance literature:: In tetrahydrofuran; a cold (-48°C) soln. of the copper reagent in dry THF was allowed to react with enone in dry THF; the mixt. was stirred under dry argon atm. at -48°C for 2 h, at -20°C for 1 h and at room temp. for 1h;; satd. aq. NH4Cl (pH 8) and diethyl ether were added and the mixt. was stirred for several min.; the organic layer was sepd., washed with satd. aq. NH4Cl and dried (MgSO4); sepn. of compds. by distn.; glc anal.; exact mass given;;