Benzenesulfonamide, 4-methyl-N-[1-[(4-methylphenyl)sulfonyl]-4-(4-nitrophenyl)-2,5-dioxo-3-(1 -piperidinyl)-4-imidazolidinyl]-

Base Information

• Chemical Name: Benzenesulfonamide, 4-methyl-N-[1-[(4-methylphenyl)sulfonyl]-4-(4-nitrophenyl)-2,5-dioxo-3-(1 -piperidinyl)-4-imidazolidinyl]-
• CAS No.: 112080-81-6
• Molecular Formula: C₂₈H₂₉N₅O₈S₂
• Molecular Weight: 627.699
• Mol file: 112080-81-6.mol

Synonyms:

Chemical Property of Benzenesulfonamide, 4-methyl-N-[1-[(4-methylphenyl)sulfonyl]-4-(4-nitrophenyl)-2,5-dioxo-3-(1 -piperidinyl)-4-imidazolidinyl]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenesulfonamide, 4-methyl-N-[1-[(4-methylphenyl)sulfonyl]-4-(4-nitrophenyl)-2,5-dioxo-3-(1 -piperidinyl)-4-imidazolidinyl]-

There total 3 articles about Benzenesulfonamide, 4-methyl-N-[1-[(4-methylphenyl)sulfonyl]-4-(4-nitrophenyl)-2,5-dioxo-3-(1 -piperidinyl)-4-imidazolidinyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

4-nitrobenzaldehyde-N,N-pentamethylene hydrazone (83785-94-8) + Tosyl isocyanate (4083-64-1) → p-Nitrophenyl-glyoxylsaeure-p-tolylsulfonamid-N,N-pentamethylenhydrazon (100010-83-1) + 5-(p-Nitro-phenyl)-1-piperidino-5-(p-tolylsulfonamido)-3-(p-tolylsulfonyl)imidazolidin-2,4-dion (112080-81-6)

Guidance literature:

In tetrachloromethane; for 672h; Ambient temperature;

DOI:10.1016/S0040-4020(01)83450-5

Reference yield:

Tosyl isocyanate (4083-64-1) → 5-(p-Nitro-phenyl)-1-piperidino-5-(p-tolylsulfonamido)-3-(p-tolylsulfonyl)imidazolidin-2,4-dion (112080-81-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 50 percent / CCl₄ / 672 h / Ambient temperature

2: 1440 h / Ambient temperature

In tetrachloromethane;

Reference yield:

Tosyl isocyanate (4083-64-1) + p-Nitrophenyl-glyoxylsaeure-p-tolylsulfonamid-N,N-pentamethylenhydrazon (100010-83-1) → 5-(p-Nitro-phenyl)-1-piperidino-5-(p-tolylsulfonamido)-3-(p-tolylsulfonyl)imidazolidin-2,4-dion (112080-81-6)

Guidance literature:

for 1440h; Ambient temperature;

upstream raw materials:

4-nitrobenzaldehyde-N,N-pentamethylene hydrazone

Tosyl isocyanate

p-Nitrophenyl-glyoxylsaeure-p-tolylsulfonamid-N,N-pentamethylenhydrazon