Technology Process of Tetracosanoic acid, 2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-, methyl
ester, (R)-
There total 6 articles about Tetracosanoic acid, 2-[[(1,1-dimethylethyl)diphenylsilyl]oxy]-, methyl
ester, (R)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 14 percent / NaOEt / ethanol / anodic coupling
2: 94 percent / MeONa / tetrahydrofuran; methanol / 16 h / 5 °C
3: 92 percent / Ph3P, diethyl azodicarboxylate / tetrahydrofuran / 1 h / 20 °C
4: 74 percent / MeONa / tetrahydrofuran; methanol / 16 h / 5 °C
5: imidazole / dimethylformamide / 24 h / 20 °C
With
1H-imidazole; sodium methylate; sodium ethanolate; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(87)80219-7
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 94 percent / MeONa / tetrahydrofuran; methanol / 16 h / 5 °C
2: 92 percent / Ph3P, diethyl azodicarboxylate / tetrahydrofuran / 1 h / 20 °C
3: 74 percent / MeONa / tetrahydrofuran; methanol / 16 h / 5 °C
4: imidazole / dimethylformamide / 24 h / 20 °C
With
1H-imidazole; sodium methylate; triphenylphosphine; diethylazodicarboxylate;
In
tetrahydrofuran; methanol; N,N-dimethyl-formamide;
DOI:10.1016/0008-6215(87)80219-7
