3-iodocholic acid

Base Information

Chemical Name:3-iodocholic acid
CAS No.:85121-73-9
Molecular Formula:C₂₄H₃₉IO₄
Molecular Weight:518.476
Hs Code.:
Mol file:85121-73-9.mol

Synonyms:3-Iodocholic acid;

Suppliers and Price of 3-iodocholic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-iodocholic acid

Chemical Property:

Vapor Pressure:6.71E-17mmHg at 25°C
Boiling Point:600°C at 760 mmHg
Flash Point:316.7°C
PSA：77.76000
Density:1.43g/cm³
LogP:4.89140

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-iodocholic acid

There total 3 articles about 3-iodocholic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 88165-74-6
7α-hydroxy-3α-iod-5β-cholansaeure-24,12α-lacton

: 85121-73-9
7α,12α-dihydroxy-3α-iod-5β-cholansaeure

Guidance literature:: With potassium hydroxide; In methanol; for 48h;
DOI:10.1016/S0040-4020(01)82452-2

Reference yield:

: 88202-27-1
7α-hydroxy-3α-phenylsulfonyloxy-5β-cholansaeure-24,12α-lacton

: 85121-73-9
7α,12α-dihydroxy-3α-iod-5β-cholansaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / NaI / acetone / 48 h / Heating

2: 83 percent / KOH / methanol / 48 h

With potassium hydroxide; sodium iodide; In methanol; acetone;
DOI:10.1016/S0040-4020(01)82452-2

Reference yield:

: 81-25-4,2464-18-8,2955-27-3,3338-16-7,10322-18-6,15073-87-7,30634-97-0,63324-19-6,63324-20-9,71883-64-2,71883-66-4,81873-90-7,81938-67-2,105227-32-5,105227-33-6,105227-34-7,105227-35-8,106927-36-0,106927-37-1,130009-06-2
cholsaeure

: 85121-73-9
7α,12α-dihydroxy-3α-iod-5β-cholansaeure

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / pyridine / 48 h / 5 °C

2: 37 percent / NaI / acetone / 48 h / Heating

3: 83 percent / KOH / methanol / 48 h

With potassium hydroxide; sodium iodide; In pyridine; methanol; acetone;
DOI:10.1016/S0040-4020(01)82452-2