3-Bromo-2,5-difluorobenzaldehyde

Base Information

• Chemical Name: 3-Bromo-2,5-difluorobenzaldehyde
• CAS No.: 112279-64-8
• Molecular Formula: C7H3BrF2O
• Molecular Weight: 221.001
• Hs Code.: 2913000090
• Mol file: 112279-64-8.mol

Synonyms:

Chemical Property of 3-Bromo-2,5-difluorobenzaldehyde

Chemical Property:

• PSA: 17.07000
• LogP: 2.53980
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

95% ^*data from raw suppliers

3-Bromo-2,5-difluorobenzaldehyde ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Bromo-2,5-difluorobenzaldehyde

There total 3 articles about 3-Bromo-2,5-difluorobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

aqueous hypophosphorous acid + 4-amino-3-bromo-2,5-difluorobenzaldehyde (112279-63-7) → 3-bromo-2,5-difluorobenzaldehyde (112279-64-8)

Guidance literature:

With acetic acid; sodium nitrite; In water;

Reference yield:

4-amino-3-bromo-2,5-difluorobenzaldehyde (112279-63-7) → 3-bromo-2,5-difluorobenzaldehyde (112279-64-8)

Guidance literature:

With hypophosphorous acid; sodium nitrite; In water; acetic acid; at 0 - 20 ℃;

Reference yield:

4-amino-3-bromo-2,5-difluorobenzonitrile (112279-62-6) → 3-bromo-2,5-difluorobenzaldehyde (112279-64-8)

Guidance literature:

With water; hypophosphorous acid; acetic acid; sodium nitrite; at 0 - 20 ℃; for 1h;

upstream raw materials:

4-amino-3-bromo-2,5-difluorobenzaldehyde

4-amino-3-bromo-2,5-difluorobenzonitrile

Downstream raw materials:

(3-bromo-2,5-difluorophenyl)methanol

C₂₂H₂₁F₂N₇O₃

4-(2,5-difluoro-3-(hydroxymethyl)phenyl)morpholin-3-one

4-(3-(bromomethyl)-2,5-difluorophenyl)morpholin-3-one

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