Technology Process of Quinoline, 6-azido-8-phenyl-
There total 5 articles about Quinoline, 6-azido-8-phenyl- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 75 percent / fuming HNO3 / acetic acid / at < 30 degC
2: 100 percent / conc. H2SO4 / 1 h / Ambient temperature
3: 63 percent / As2O5, conc. H2SO4 / 4 h / 160 °C
4: 100 percent / H2 / 10 percent Pd-C / ethanol
5: 1.) NaNO2, HCl, 2.) NaN3, NaOAc
With
hydrogenchloride; sodium azide; arsenic(V) oxide; sulfuric acid; hydrogen; nitric acid; sodium acetate; sodium nitrite;
palladium on activated charcoal;
In
ethanol; acetic acid;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 63 percent / As2O5, conc. H2SO4 / 4 h / 160 °C
2: 100 percent / H2 / 10 percent Pd-C / ethanol
3: 1.) NaNO2, HCl, 2.) NaN3, NaOAc
With
hydrogenchloride; sodium azide; arsenic(V) oxide; sulfuric acid; hydrogen; sodium acetate; sodium nitrite;
palladium on activated charcoal;
In
ethanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 100 percent / conc. H2SO4 / 1 h / Ambient temperature
2: 63 percent / As2O5, conc. H2SO4 / 4 h / 160 °C
3: 100 percent / H2 / 10 percent Pd-C / ethanol
4: 1.) NaNO2, HCl, 2.) NaN3, NaOAc
With
hydrogenchloride; sodium azide; arsenic(V) oxide; sulfuric acid; hydrogen; sodium acetate; sodium nitrite;
palladium on activated charcoal;
In
ethanol;
