dibenzyl piperazine-1,4-dicarbodithioate

Base Information

Chemical Name:dibenzyl piperazine-1,4-dicarbodithioate
CAS No.:21585-27-3
Molecular Formula:C20H22 N2 S4
Molecular Weight:418.672
Hs Code.:
Mol file:21585-27-3.mol

Synonyms:1,4-Piperazinedicarbodithioicacid, bis(phenylmethyl) ester (9CI); 1,4-Piperazinedicarbodithioic acid,dibenzyl ester (6CI,8CI); Dibenzyl 1,4-piperazinedicarbodithioate; NSC 318151

Suppliers and Price of dibenzyl piperazine-1,4-dicarbodithioate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of dibenzyl piperazine-1,4-dicarbodithioate

Chemical Property:

Vapor Pressure:1.21E-12mmHg at 25°C
Boiling Point:561.7°Cat760mmHg
Flash Point:293.5°C
Density:1.324g/cm³

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of dibenzyl piperazine-1,4-dicarbodithioate

There total 9 articles about dibenzyl piperazine-1,4-dicarbodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 3012-37-1
benzyl thiocyanate

: bis(piperazinium)piperazine-1,4-dicarbodithioate

: 21585-27-3
dibenzyl piperazine-1,4-bis(carbodithioate)

Guidance literature:: With sodium dodecyl-sulfate; In water; at 20 ℃; for 3h;
DOI:10.1080/17415993.2016.1166225

Reference yield: 51.2%

: 1605349-68-5
sodium 4-(benzylthiocarbonothioyl)piperazine-1-carbodithioate

: 100-44-7
benzyl chloride

: 109400-03-5
benzyl 4-benzylpiperazine-1-carbodithioate

: 21585-27-3
dibenzyl piperazine-1,4-bis(carbodithioate)

Guidance literature:: With triethylamine; In methanol; at 20 ℃; for 3h;
DOI:10.1039/c4ob00005f

Reference yield:

: 1605349-59-4
tert-butyl 4-(benzylthiocarbonothioyl)piperazine-1-carboxylate

: 109400-03-5
benzyl 4-benzylpiperazine-1-carbodithioate

: 21585-27-3
dibenzyl piperazine-1,4-bis(carbodithioate)

Guidance literature:: Multi-step reaction with 3 steps

1.1: trifluoroacetic acid / dichloromethane / 6 h / 0 - 20 °C

1.2: 4 h / 0 - 20 °C

2.1: sodium hydroxide / ethyl acetate; water / 10 h / 5 - 20 °C

3.1: triethylamine / methanol / 3 h / 20 °C

With triethylamine; trifluoroacetic acid; sodium hydroxide; In methanol; dichloromethane; water; ethyl acetate;
DOI:10.1039/c4ob00005f