3,5-Octadiyne-2,7-diol

Base Information

Chemical Name:3,5-Octadiyne-2,7-diol
CAS No.:14400-73-8
Molecular Formula:C8H10 O2
Molecular Weight:138.1638
Hs Code.:
NSC Number:172807
DSSTox Substance ID:DTXSID30305939
Nikkaji Number:J803.462A
Mol file:14400-73-8.mol

Synonyms:3,5-octadiyne-2,7-diol;14400-73-8;NSC172807;SCHEMBL11823906;DTXSID30305939;NSC-172807

Suppliers and Price of 3,5-Octadiyne-2,7-diol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 3,5-Octadiyne-2,7-diol

Chemical Property:

Vapor Pressure:0.000824mmHg at 25°C
Boiling Point:271.7°C at 760 mmHg
Flash Point:131.6°C
Density:1.123g/cm³
XLogP3:0.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:138.068079557
Heavy Atom Count:10
Complexity:191

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C#CC#CC(C)O)O

Technology Process of 3,5-Octadiyne-2,7-diol

There total 14 articles about 3,5-Octadiyne-2,7-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 2028-63-9
but-3-yn-2-ol

: 14400-73-8
octa-3,5-diyne-2,7-diol

Guidance literature:: With copper(l) iodide; nickel(II) chloride hexahydrate; N,N,N,N,-tetramethylethylenediamine; In tetrahydrofuran; at 20 ℃; for 1h; Inert atmosphere; Darkness;
DOI:10.1039/c3ra46491a

Reference yield: 58.0%

: 1262958-22-4
2-iodo-3,5,6-trimethoxytoluene

: 2028-63-9
but-3-yn-2-ol

: 14400-73-8
octa-3,5-diyne-2,7-diol

: 1551325-18-8
4-(3,4,6-trimethoxy-2-methylphenyl)but-3-yn-2-ol

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diethylamine; In dimethyl sulfoxide; at 65 - 75 ℃; for 16h; Overall yield = 44 %Spectr.; Inert atmosphere;
DOI:10.1039/c3ob42333f

Reference yield:

: 2060-24-4
4-bromo-3-butyn-2-ol

: 2028-63-9
but-3-yn-2-ol

: 14400-73-8
octa-3,5-diyne-2,7-diol

Guidance literature:: With N-butylamine; copper(l) chloride; hydroxylamine hydrochloride; In dichloromethane; water; at 0 - 20 ℃;
DOI:10.1021/ja0719430