Carbamimidothioic acid, [(dimethylamino)methylene](4-methylphenyl)-,methyl ester

Base Information

• Chemical Name: Carbamimidothioic acid, [(dimethylamino)methylene](4-methylphenyl)-,methyl ester
• CAS No.: 112519-67-2
• Molecular Formula: C12H17N3S
• Molecular Weight: 235.353

Synonyms:Carbamimidothioic acid, [(dimethylamino)methylene](4-methylphenyl)-,methyl ester

Chemical Property of Carbamimidothioic acid, [(dimethylamino)methylene](4-methylphenyl)-,methyl ester

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

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Technology Process of Carbamimidothioic acid, [(dimethylamino)methylene](4-methylphenyl)-,methyl ester

There total 3 articles about Carbamimidothioic acid, [(dimethylamino)methylene](4-methylphenyl)-,methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

4-dimethylamino-2-methylsulfanyl-1-p-tolyl-1,3-diazabuta-1,3-dienium iodide (112519-78-5) → 4-dimethylamino-2-methylsulfanyl-1-p-tolyl-1,3-diazabuta-1,3-diene (112519-67-2)

Guidance literature:

With potassium hydrogencarbonate; In diethyl ether; water; at 20 ℃; for 2h; Saturated solution;

DOI:10.1016/j.tet.2010.10.059

Reference yield:

1-[1-Dimethylamino-meth-(E)-ylidene]-3-p-tolyl-thiourea (112519-75-2) + methyl iodide (74-88-4) → 1-p-tolyl-4-dimethylamino-2-thiomethyl-1,3-diazabutadiene (112519-67-2)

Guidance literature:

In acetone; Ambient temperature;

DOI:10.1016/S0040-4039(00)96169-0

Reference yield:

4-dimethylamino-2-p-tolylamino-1,3-thiazabuta-1,3-diene (112519-75-2) + methyl iodide (74-88-4) → 4-dimethylamino-2-methylsulfanyl-1-p-tolyl-1,3-diazabuta-1,3-diene (112519-67-2)

Guidance literature:

With potassium hydroxide; Yield given. Multistep reaction; 1) acetone, RT, 10 h;

DOI:10.1055/s-1990-26892

upstream raw materials:

4-dimethylamino-2-p-tolylamino-1,3-thiazabuta-1,3-diene

methyl iodide

4-dimethylamino-2-methylsulfanyl-1-p-tolyl-1,3-diazabuta-1,3-dienium iodide

1-[1-Dimethylamino-meth-(E)-ylidene]-3-p-tolyl-thiourea

Downstream raw materials:

5-p-chlorobenzoylamino-4-dimethylamino-5-methyl-2-methylthio-1-p-tolyl-1,4,5,6-tetrahydropyrimidin-6-one

5-phenyl-2-methylthio-1-p-tolyl-1,6-dihydropyrimidin-6-one

5-chloro-2-methylthio-1-p-tolyl-1,6-dihydropyrimidin-6-one

2-p-tolyl-5-dimethylamino-3-thiomethyl-1,2,4-thiadiazine-1,1-dioxide

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