6H-Azocino[4,3-b]indol-6-one, 1,2,3,4,5,7-hexahydro-2-(phenylmethyl)-7-(phenylsulfonyl)-

Base Information

Chemical Name:6H-Azocino[4,3-b]indol-6-one, 1,2,3,4,5,7-hexahydro-2-(phenylmethyl)-7-(phenylsulfonyl)-
CAS No.:112565-49-8
Molecular Formula:C₂₆H₂₄N₂O₃S
Molecular Weight:444.554
Hs Code.:

Synonyms:

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Chemical Property of 6H-Azocino[4,3-b]indol-6-one, 1,2,3,4,5,7-hexahydro-2-(phenylmethyl)-7-(phenylsulfonyl)-

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Technology Process of 6H-Azocino[4,3-b]indol-6-one, 1,2,3,4,5,7-hexahydro-2-(phenylmethyl)-7-(phenylsulfonyl)-

There total 5 articles about 6H-Azocino[4,3-b]indol-6-one, 1,2,3,4,5,7-hexahydro-2-(phenylmethyl)-7-(phenylsulfonyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 40899-71-6
1-benzenesulfonylindole

: 112565-49-8
2-benzyl-1,2,3,4-tetrahydro-7-phenylsulphonylazocino-<4,3-b>indol-6 (5 H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / butyl-lithium / tetrahydrofuran / 1.5 h / Ambient temperature

2: 63 percent / lithium aluminium hydride / tetrahydrofuran / 12 h / Heating

3: 96 percent / acetic acid; 1,2-dimethoxy-ethane / 0.33 h / Ambient temperature

4: 53 percent / manganese dioxide / CHCl₃ / 48 h / Ambient temperature

5: 82 percent / 50percent aq. sodium hydroxide, tetrabutylammonium hydroxide / benzene / 1 h

With manganese(IV) oxide; sodium hydroxide; lithium aluminium tetrahydride; n-butyllithium; tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; chloroform; acetic acid; benzene;
DOI:10.1039/P19870001599

Reference yield:

: 2399-66-8
1-benzoylpyrrolidin-2-one

: 112565-49-8
2-benzyl-1,2,3,4-tetrahydro-7-phenylsulphonylazocino-<4,3-b>indol-6 (5 H)-one

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / butyl-lithium / tetrahydrofuran / 1.5 h / Ambient temperature

2: 63 percent / lithium aluminium hydride / tetrahydrofuran / 12 h / Heating

3: 96 percent / acetic acid; 1,2-dimethoxy-ethane / 0.33 h / Ambient temperature

4: 53 percent / manganese dioxide / CHCl₃ / 48 h / Ambient temperature

5: 82 percent / 50percent aq. sodium hydroxide, tetrabutylammonium hydroxide / benzene / 1 h

With manganese(IV) oxide; sodium hydroxide; lithium aluminium tetrahydride; n-butyllithium; tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; chloroform; acetic acid; benzene;
DOI:10.1039/P19870001599

Reference yield:

: 112565-46-5
4-benzylamino-1-indol-2-ylbutan-1-ol

: 112565-49-8
2-benzyl-1,2,3,4-tetrahydro-7-phenylsulphonylazocino-<4,3-b>indol-6 (5 H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / acetic acid; 1,2-dimethoxy-ethane / 0.33 h / Ambient temperature

2: 53 percent / manganese dioxide / CHCl₃ / 48 h / Ambient temperature

3: 82 percent / 50percent aq. sodium hydroxide, tetrabutylammonium hydroxide / benzene / 1 h

With manganese(IV) oxide; sodium hydroxide; tetra(n-butyl)ammonium hydroxide; In 1,2-dimethoxyethane; chloroform; acetic acid; benzene;
DOI:10.1039/P19870001599