Diindolo[3,2,1-de:3',2',1'-ij][1,5]naphthyridine-6,13-dione, 7,14-diphenyl-

Base Information

Chemical Name:Diindolo[3,2,1-de:3',2',1'-ij][1,5]naphthyridine-6,13-dione, 7,14-diphenyl-
CAS No.:6417-51-2
Molecular Formula:C32H18 N2 O2
Molecular Weight:462.507
Hs Code.:2933990090
DSSTox Substance ID:DTXSID9064346
Nikkaji Number:J93.167E
Mol file:6417-51-2.mol

Synonyms:6417-51-2;Diindolo[3,2,1-de:3',2',1'-ij][1,5]naphthyridine-6,13-dione, 7,14-diphenyl-;Diindolo(3,2,1-de:3',2',1'-ij)(1,5)naphthyridine-6,13-dione, 7,14-diphenyl-;EINECS 229-141-8;DTXSID9064346;SCHEMBL14411287;C.I.73095

Suppliers and Price of Diindolo[3,2,1-de:3',2',1'-ij][1,5]naphthyridine-6,13-dione, 7,14-diphenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of Diindolo[3,2,1-de:3',2',1'-ij][1,5]naphthyridine-6,13-dione, 7,14-diphenyl-

Chemical Property:

Boiling Point:701.2±60.0 °C(Predicted)
PKA:-1.27±0.60(Predicted)
PSA：109.39000
Density:1.50±0.1 g/cm3(Predicted)
LogP:0.64180
XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:462.136827821
Heavy Atom Count:36
Complexity:1010

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C3C4=CC=CC=C4N5C3=C6C(=C(C5=O)C7=CC=CC=C7)C8=CC=CC=C8N6C2=O

Technology Process of Diindolo[3,2,1-de:3',2',1'-ij][1,5]naphthyridine-6,13-dione, 7,14-diphenyl-

There total 7 articles about Diindolo[3,2,1-de:3',2',1'-ij][1,5]naphthyridine-6,13-dione, 7,14-diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 103-80-0
phenylacetyl chloride

: 64784-13-0,482-89-3,141901-19-1,12626-73-2
indigo

: 6417-51-2
7,14-diphenyl-diindolo[3,2,1-de;3',2',1'-ij][1,5]naphthyridine-6,13-dione

Guidance literature:: In 5,5-dimethyl-1,3-cyclohexadiene; at 140 ℃; for 48h; Inert atmosphere;
DOI:10.1016/j.molstruc.2018.07.009

Reference yield:

: 552-89-6
2-nitro-benzaldehyde

: 6417-51-2
7,14-diphenyl-diindolo[3,2,1-de;3',2',1'-ij][1,5]naphthyridine-6,13-dione

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / acetone; water / -5 - 20 °C / pH 10

2: 5,5-dimethyl-1,3-cyclohexadiene / 48 h / 140 °C / Inert atmosphere

With sodium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; water; acetone;
DOI:10.1016/j.molstruc.2018.07.009