1-Azetidinesulfonic acid, 2-oxo-3-[2-oxo-2-[(phenylmethyl)amino]ethyl]-4-(2-phenylethyl)-, monopotassium salt, cis-

Base Information

Chemical Name:1-Azetidinesulfonic acid, 2-oxo-3-[2-oxo-2-[(phenylmethyl)amino]ethyl]-4-(2-phenylethyl)-, monopotassium salt, cis-
CAS No.:112634-23-8
Molecular Formula:C₂₀H₂₁N₂O₅S*K
Molecular Weight:440.561
Hs Code.:

Synonyms:

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Chemical Property of 1-Azetidinesulfonic acid, 2-oxo-3-[2-oxo-2-[(phenylmethyl)amino]ethyl]-4-(2-phenylethyl)-, monopotassium salt, cis-

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Technology Process of 1-Azetidinesulfonic acid, 2-oxo-3-[2-oxo-2-[(phenylmethyl)amino]ethyl]-4-(2-phenylethyl)-, monopotassium salt, cis-

There total 7 articles about 1-Azetidinesulfonic acid, 2-oxo-3-[2-oxo-2-[(phenylmethyl)amino]ethyl]-4-(2-phenylethyl)-, monopotassium salt, cis- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 14371-10-9
(E)-3-phenylpropenal

: 112634-23-8
Potassium; 3-(benzylcarbamoyl-methyl)-2-oxo-4-phenethyl-azetidine-1-sulfonate

Guidance literature:: Multi-step reaction with 7 steps

2: 52 percent / cyanuric chloride, triethylamine / CH₂Cl₂ / 1.) -40 deg C, 4 h, 2.) -40 to -18 deg C, overnight

3: 61 percent / trifluoroacetic acid / ethanol; H₂O / 72 h / 40 °C

4: 65 percent / ceric ammonium nitrate / acetonitrile; H₂O / 0.5 h / -10 °C

5: 87 percent / 2 h / 70 °C

6: 56 percent / H₂ / platinum / ethanol / 0.5 h / at normal pressure

7: 1.) pyridine sulfur trioxide complex, 2.) Dowex 50X₈-200 ion exchange resin (potassium form) / 1.) pyridine, 80 deg C, 2 h

With 1,3,5-trichloro-2,4,6-triazine; ammonium cerium(IV) nitrate; Dowex 50X₈-200 ion exchange resin (potassium form); hydrogen; sulfur trioxide pyridine complex; triethylamine; trifluoroacetic acid; platinum; In ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 88315-63-3
(E)-4-methoxy-N-((E)-3-phenylallylidene)aniline

: 112634-23-8
Potassium; 3-(benzylcarbamoyl-methyl)-2-oxo-4-phenethyl-azetidine-1-sulfonate

Guidance literature:: Multi-step reaction with 6 steps

1: 52 percent / cyanuric chloride, triethylamine / CH₂Cl₂ / 1.) -40 deg C, 4 h, 2.) -40 to -18 deg C, overnight

2: 61 percent / trifluoroacetic acid / ethanol; H₂O / 72 h / 40 °C

3: 65 percent / ceric ammonium nitrate / acetonitrile; H₂O / 0.5 h / -10 °C

4: 87 percent / 2 h / 70 °C

5: 56 percent / H₂ / platinum / ethanol / 0.5 h / at normal pressure

6: 1.) pyridine sulfur trioxide complex, 2.) Dowex 50X₈-200 ion exchange resin (potassium form) / 1.) pyridine, 80 deg C, 2 h

With 1,3,5-trichloro-2,4,6-triazine; ammonium cerium(IV) nitrate; Dowex 50X₈-200 ion exchange resin (potassium form); hydrogen; sulfur trioxide pyridine complex; triethylamine; trifluoroacetic acid; platinum; In ethanol; dichloromethane; water; acetonitrile;

Reference yield:

: 112634-10-3
[2-Oxo-4-((E)-styryl)-azetidin-3-yl]-thioacetic acid S-ethyl ester

: 112634-23-8
Potassium; 3-(benzylcarbamoyl-methyl)-2-oxo-4-phenethyl-azetidine-1-sulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / 2 h / 70 °C

2: 56 percent / H₂ / platinum / ethanol / 0.5 h / at normal pressure

3: 1.) pyridine sulfur trioxide complex, 2.) Dowex 50X₈-200 ion exchange resin (potassium form) / 1.) pyridine, 80 deg C, 2 h

With Dowex 50X₈-200 ion exchange resin (potassium form); hydrogen; sulfur trioxide pyridine complex; platinum; In ethanol;