Technology Process of Benzoic acid, 2,4-dihydroxy-6-[(2-pentyl-1,3-dioxolan-2-yl)methyl]-, ethyl
ester
There total 7 articles about Benzoic acid, 2,4-dihydroxy-6-[(2-pentyl-1,3-dioxolan-2-yl)methyl]-, ethyl
ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 60 percent / pyridinium chlorochromate / CH2Cl2 / 2 h
2: 69 percent / toluene / 20 h / Heating
3: 55 percent / ethanol / 24 h / Heating
4: acetic acid / 0.5 h / Heating
With
pyridinium chlorochromate;
In
ethanol; dichloromethane; acetic acid; toluene;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 82 percent / lithium aluminium hydride / diethyl ether / 4 h / Heating
2: 60 percent / pyridinium chlorochromate / CH2Cl2 / 2 h
3: 69 percent / toluene / 20 h / Heating
4: 55 percent / ethanol / 24 h / Heating
5: acetic acid / 0.5 h / Heating
With
lithium aluminium tetrahydride; pyridinium chlorochromate;
In
diethyl ether; ethanol; dichloromethane; acetic acid; toluene;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 69 percent / p-toluenesulfonic acid / toluene / 6 h / Heating
2: 82 percent / lithium aluminium hydride / diethyl ether / 4 h / Heating
3: 60 percent / pyridinium chlorochromate / CH2Cl2 / 2 h
4: 69 percent / toluene / 20 h / Heating
5: 55 percent / ethanol / 24 h / Heating
6: acetic acid / 0.5 h / Heating
With
lithium aluminium tetrahydride; toluene-4-sulfonic acid; pyridinium chlorochromate;
In
diethyl ether; ethanol; dichloromethane; acetic acid; toluene;
