Technology Process of Benzoic acid,
2-hydroxy-6-(2-oxoheptyl)-4-[[2-[(2-pentyl-1,3-dioxolan-2-yl)methyl]-4,6-
bis(phenylmethoxy)benzoyl]oxy]-, phenylmethyl ester
There total 10 articles about Benzoic acid,
2-hydroxy-6-(2-oxoheptyl)-4-[[2-[(2-pentyl-1,3-dioxolan-2-yl)methyl]-4,6-
bis(phenylmethoxy)benzoyl]oxy]-, phenylmethyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dicyclohexyl-carbodiimide;
In
diethyl ether;
for 2h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 9 steps
1: 82 percent / lithium aluminium hydride / diethyl ether / 4 h / Heating
2: 60 percent / pyridinium chlorochromate / CH2Cl2 / 2 h
3: 69 percent / toluene / 20 h / Heating
4: 55 percent / ethanol / 24 h / Heating
5: acetic acid / 0.5 h / Heating
7: 38 percent / phenylmethanol / 24 h / 130 °C
8: 97 percent / p-toluenesulfonic acid / acetone / 10 h / Ambient temperature
9: 12 percent / dicyclohexylcarbodiimide / diethyl ether / 2 h / Ambient temperature
With
lithium aluminium tetrahydride; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; pyridinium chlorochromate;
In
diethyl ether; ethanol; dichloromethane; acetic acid; acetone; toluene; benzyl alcohol;
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 69 percent / toluene / 20 h / Heating
2: 55 percent / ethanol / 24 h / Heating
3: acetic acid / 0.5 h / Heating
5: 38 percent / phenylmethanol / 24 h / 130 °C
6: 97 percent / p-toluenesulfonic acid / acetone / 10 h / Ambient temperature
7: 12 percent / dicyclohexylcarbodiimide / diethyl ether / 2 h / Ambient temperature
With
toluene-4-sulfonic acid; dicyclohexyl-carbodiimide;
In
diethyl ether; ethanol; acetic acid; acetone; toluene; benzyl alcohol;
