2,2-Dibromo-1-cyclohexylethan-1-one

Base Information

Chemical Name:2,2-Dibromo-1-cyclohexylethan-1-one
CAS No.:112741-18-1
Molecular Formula:C8H12Br2O
Molecular Weight:283.991
Hs Code.:
DSSTox Substance ID:DTXSID30499387
Wikidata:Q82350121

Synonyms:112741-18-1;2,2-Dibromo-1-cyclohexylethan-1-one;di-bromoacetylcyclohexane;DTXSID30499387

Suppliers and Price of 2,2-Dibromo-1-cyclohexylethan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2,2-Dibromo-1-cyclohexylethan-1-one

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:283.92344
Heavy Atom Count:11
Complexity:139

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)C(=O)C(Br)Br

Technology Process of 2,2-Dibromo-1-cyclohexylethan-1-one

There total 7 articles about 2,2-Dibromo-1-cyclohexylethan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 931-48-6
2-cyclohexylacetylene

: 112741-18-1
2,2-dibromo-1-cyclohexyl-1-ethanone

Guidance literature:: With N,N'-ethylenethiourea; 1,3-dibromo-5,5-dimethylhydantoin; water; at 20 ℃;
DOI:10.1039/c7gc00283a

Reference yield:

: 81060-37-9
(cyclohexylcarbonyl)dibromomethane

: 112741-18-1
2,2-dibromo-1-cyclohexyl-1-ethanone

Guidance literature:: With 4 A molecular sieve; pyridinium chlorochromate; In dichloromethane; for 48h; Yield given; Ambient temperature;
DOI:10.1021/jo00241a020

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 112741-18-1
2,2-dibromo-1-cyclohexyl-1-ethanone

Guidance literature:: Multi-step reaction with 2 steps

1: lithium dicyclohexylamide / tetrahydrofuran / 1 h / -78 °C

2: PCC, molecular sieves 4A / CH₂Cl₂ / 48 h / Ambient temperature

With 4 A molecular sieve; lithium dicyclohexylamide; pyridinium chlorochromate; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jo00241a020