Benzoic acid, 5-(aminosulfonyl)-2-butoxy-4-chloro-

Base Information

Chemical Name:Benzoic acid, 5-(aminosulfonyl)-2-butoxy-4-chloro-
CAS No.:112767-61-0
Molecular Formula:C₁₁H₁₄ClNO₅S
Molecular Weight:307.755
Hs Code.:

Synonyms:

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Chemical Property of Benzoic acid, 5-(aminosulfonyl)-2-butoxy-4-chloro-

Chemical Property:

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Technology Process of Benzoic acid, 5-(aminosulfonyl)-2-butoxy-4-chloro-

There total 9 articles about Benzoic acid, 5-(aminosulfonyl)-2-butoxy-4-chloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52873-25-3
4-Chlorosalicylic acid ethyl ester

: 112767-61-0
2-Butoxy-4-chloro-5-sulfamoylsalicylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) K₂CO₃ / 1.) acetone, 2.) reflux, 12 h

2: 95 percent / 30percent KOH / 1 h / Heating

3: 83 percent / 57percent HNO₃, conc. H₂SO₄ / 2 h

4: 90 percent / H₂ / 10percent Pd/C / aq. NaOH / 20 °C / 836 Torr

With potassium hydroxide; sulfuric acid; hydrogen; nitric acid; potassium carbonate; palladium on activated charcoal; In sodium hydroxide;
DOI:10.1007/BF01145556

Reference yield:

: 5106-98-9
4-chlorosalicylic acid

: 112767-61-0
2-Butoxy-4-chloro-5-sulfamoylsalicylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) K₂CO₃ / 1.) acetone, 2.) reflux, 12 h

2: 95 percent / 30percent KOH / 1 h / Heating

3: 83 percent / 57percent HNO₃, conc. H₂SO₄ / 2 h

4: 90 percent / H₂ / 10percent Pd/C / aq. NaOH / 20 °C / 836 Torr

With potassium hydroxide; sulfuric acid; hydrogen; nitric acid; potassium carbonate; palladium on activated charcoal; In sodium hydroxide;
DOI:10.1007/BF01145556

Reference yield:

: 112767-60-9
2-Butoxy-4-chlorobenzoic acid

: 112767-61-0
2-Butoxy-4-chloro-5-sulfamoylsalicylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / 57percent HNO₃, conc. H₂SO₄ / 2 h

2: 90 percent / H₂ / 10percent Pd/C / aq. NaOH / 20 °C / 836 Torr

With sulfuric acid; hydrogen; nitric acid; palladium on activated charcoal; In sodium hydroxide;
DOI:10.1007/BF01145556