Propanedioic acid, [1-methyl-2-(phenylsulfonyl)ethylidene]-, dimethyl ester

Base Information

Chemical Name:Propanedioic acid, [1-methyl-2-(phenylsulfonyl)ethylidene]-, dimethyl ester
CAS No.:112841-16-4
Molecular Formula:C14H16O6S
Molecular Weight:312.343
Hs Code.:

Synonyms:

Suppliers and Price of Propanedioic acid, [1-methyl-2-(phenylsulfonyl)ethylidene]-, dimethyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Propanedioic acid, [1-methyl-2-(phenylsulfonyl)ethylidene]-, dimethyl ester

Chemical Property:

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Technology Process of Propanedioic acid, [1-methyl-2-(phenylsulfonyl)ethylidene]-, dimethyl ester

There total 4 articles about Propanedioic acid, [1-methyl-2-(phenylsulfonyl)ethylidene]-, dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 112841-15-3
methyl 2-carbomethoxy-3-<(phenylsulfonyl)methyl>-3-butenoate

: 112841-16-4
methyl 2-carbomethoxy-3-<(phenylsulfonyl)methyl>-2-butenoate

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 25 ℃; for 12h;
DOI:10.1021/jo00022a032

Reference yield:

: 108-59-8
malonic acid dimethyl ester

: 112841-16-4
methyl 2-carbomethoxy-3-<(phenylsulfonyl)methyl>-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium hydride

2: potassium tert-butoxide / tetrahydrofuran

With potassium tert-butylate; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja00213a042

Reference yield:

: (phenylsulfonyl)allene

: 112841-16-4
methyl 2-carbomethoxy-3-<(phenylsulfonyl)methyl>-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / sodium hydride

2: potassium tert-butoxide / tetrahydrofuran

With potassium tert-butylate; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja00213a042