Technology Process of 4-t-Butyl-1-oxo-1-phospha-2,6,7-trioxabicyclo(2.2.2)octane
There total 9 articles about 4-t-Butyl-1-oxo-1-phospha-2,6,7-trioxabicyclo(2.2.2)octane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfuryl dichloride;
In
chloroform;
for 2h;
- Guidance literature:
-
With
pyridine; trichlorophosphate;
In
acetonitrile;
1.) r.t., 12 h, 2.) 50 deg C, 5 h;
DOI:10.1271/bbb1961.46.411
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 65 percent / formic acid, hydrogen peroxide
2: 70 percent / periodic acid / H2O; methanol
3: 23 percent / calcium oxide / H2O / 1.) 3 h, room temperature, 2.) 35 h, 70-80 deg C
4: 79 percent / triethylphosphite, triethylamine / ethanol / Heating
5: 86 percent / sulphuryl chloride / CHCl3 / 2 h
With
formic acid; sulfuryl dichloride; dihydrogen peroxide; periodic acid; triethylamine; triethyl phosphite;
calcium oxide;
In
methanol; ethanol; chloroform; water;