Benzene, 1-bromo-3-fluoro-5-(1-methylethyl)-

Base Information

Chemical Name:Benzene, 1-bromo-3-fluoro-5-(1-methylethyl)-
CAS No.:112930-19-5
Molecular Formula:C₉H₁₀BrF
Molecular Weight:217.081
Hs Code.:

Synonyms:

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Chemical Property of Benzene, 1-bromo-3-fluoro-5-(1-methylethyl)-

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Technology Process of Benzene, 1-bromo-3-fluoro-5-(1-methylethyl)-

There total 5 articles about Benzene, 1-bromo-3-fluoro-5-(1-methylethyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₉H₁₀Br₂Mg

: 112930-19-5
3-bromo-5-fluorocumene

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) magnesium, iodine, 2.) hydrochloric acid (3M) / 1.) ether, reflux, 2.) ether, overnight

2: thionyl chloride / 5 h / Heating

3: 1.) sodium azide (20percent) / 1.) acetone, from 0 deg C to RT, 10 min, 2.) reflux, 5 h

4: 100 percent / hydrochloric acid (3M) / ethanol / 2 h / Heating

5: 1.) hydrochloric acid (3M), sodium nitrite, ammonium hexafluorophosphate / 1.) water, 0 deg C, 2.) heating, 10 min

With hydrogenchloride; ammonium hexafluorophosphate; thionyl chloride; sodium azide; iodine; magnesium; sodium nitrite; In ethanol;

Reference yield:

: 112930-39-9
3-bromo-5-isopropylbenzoic acid

: 112930-19-5
3-bromo-5-fluorocumene

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / 5 h / Heating

2: 1.) sodium azide (20percent) / 1.) acetone, from 0 deg C to RT, 10 min, 2.) reflux, 5 h

3: 100 percent / hydrochloric acid (3M) / ethanol / 2 h / Heating

4: 1.) hydrochloric acid (3M), sodium nitrite, ammonium hexafluorophosphate / 1.) water, 0 deg C, 2.) heating, 10 min

With hydrogenchloride; ammonium hexafluorophosphate; thionyl chloride; sodium azide; sodium nitrite; In ethanol;

Reference yield:

: 849934-90-3
3-bromo-5-isopropyl-benzoyl chloride

: 112930-19-5
3-bromo-5-fluorocumene

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) sodium azide (20percent) / 1.) acetone, from 0 deg C to RT, 10 min, 2.) reflux, 5 h

2: 100 percent / hydrochloric acid (3M) / ethanol / 2 h / Heating

3: 1.) hydrochloric acid (3M), sodium nitrite, ammonium hexafluorophosphate / 1.) water, 0 deg C, 2.) heating, 10 min

With hydrogenchloride; ammonium hexafluorophosphate; sodium azide; sodium nitrite; In ethanol;