2,4,6-Triphenyl-1,3-azaphosphinine

Base Information

• Chemical Name: 2,4,6-Triphenyl-1,3-azaphosphinine
• CAS No.: 113035-95-3
• Molecular Formula: C22H16NP
• Molecular Weight: 325.35
• DSSTox Substance ID: DTXSID40548714
• Wikidata: Q82427511

Synonyms:2,4,6-Triphenyl-1,3-azaphosphinine;113035-95-3;DTXSID40548714

Chemical Property of 2,4,6-Triphenyl-1,3-azaphosphinine

Chemical Property:

• XLogP3: 5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 3
• Exact Mass: 325.102036512
• Heavy Atom Count: 24
• Complexity: 366

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C2=CC(=PC(=N2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 2,4,6-Triphenyl-1,3-azaphosphinine

There total 1 articles about 2,4,6-Triphenyl-1,3-azaphosphinine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

Tris(trimethylsilyl)phosphane (15573-38-3) + 2,4,6-triphenyl-1,3-oxazinium tetrafluoroborate → 2,4,6-triphenyl-1,3λ3-azaphosphinin (113035-95-3)

Guidance literature:

In acetonitrile; for 12h; Heating;

DOI:10.1016/S0040-4039(00)95919-7

Reference yield: 85.0%

1,4-bis(trimethylsilyl)-1,3-butadiyne (4526-07-2) + 2,4,6-triphenyl-1,3λ3-azaphosphinin (113035-95-3) → 4,6,4',6'-Tetraphenyl-2,2'-bis-trimethylsilanyl-[3,3']biphosphininyl

Guidance literature:

In toluene; at 90 ℃; under 600048 Torr;

DOI:10.1016/0040-4039(95)00636-Q

Reference yield: 77.0%

2,4-hexadiyne (2809-69-0) + 2,4,6-triphenyl-1,3λ3-azaphosphinin (113035-95-3) → 2,2'-Dimethyl-4,6,4',6'-tetraphenyl-[3,3']biphosphininyl

Guidance literature:

In toluene; at 90 ℃; under 600048 Torr;

DOI:10.1016/0040-4039(95)00636-Q

upstream raw materials:

Tris(trimethylsilyl)phosphane

Downstream raw materials:

C₄₅H₃₄N₂P₂

2-Diphenylphosphanyl-3,4,6-triphenyl-phosphinine

2-(Diphenyl-phosphinoyl)-3,4,6-triphenyl-phosphinine

9-Aza-2,4,6-triphosphatetracyclo<5.3.0.0^2,4.0^3,6>deca-8,10(1)-dien

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