Benzene, 1-methyl-2-(3-methylphenoxy)-

Base Information

Chemical Name:Benzene, 1-methyl-2-(3-methylphenoxy)-
CAS No.:66658-61-5
Molecular Formula:C14H14O
Molecular Weight:198.265
Hs Code.:
DSSTox Substance ID:DTXSID80216829
Wikidata:Q83093137

Synonyms:Benzene, 1-methyl-2-(3-methylphenoxy)-;66658-61-5;1-methyl-2-(3-methylphenoxy)benzene;1-methyl-3-(2-methylphenoxy)benzene;SCHEMBL2842257;DTXSID80216829;MFCD31010295

Suppliers and Price of Benzene, 1-methyl-2-(3-methylphenoxy)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Benzene, 1-methyl-2-(3-methylphenoxy)-

Chemical Property:

Vapor Pressure:0.00648mmHg at 25°C
Boiling Point:280.3°Cat760mmHg
Flash Point:118°C
Density:1.029g/cm³
XLogP3:4.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:198.104465066
Heavy Atom Count:15
Complexity:190

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)OC2=CC=CC=C2C

Technology Process of Benzene, 1-methyl-2-(3-methylphenoxy)-

There total 7 articles about Benzene, 1-methyl-2-(3-methylphenoxy)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: bis(2-methylphenyl)iodonium tetrafluoroborate

: 108-39-4
3-methyl-phenol

: 66658-61-5
1-methyl-2-(m-tolyloxy)benzene

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 40 ℃;
DOI:10.1002/chem.201703057

Reference yield: 50.0%

: 615-37-2
ortho-methylphenyl iodide

: 108-39-4
3-methyl-phenol

: 66658-61-5
1-methyl-2-(m-tolyloxy)benzene

Guidance literature:: With copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 24h; Air;
DOI:10.1055/s-0031-1290110

Reference yield:

: 16419-60-6
2-Methylphenylboronic acid

: 66658-61-5
1-methyl-2-(m-tolyloxy)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.5 h / 0 - 20 °C

1.2: 0.25 h / 20 °C

2.1: potassium tert-butylate / tetrahydrofuran / 40 °C

With potassium tert-butylate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1002/chem.201703057