Tributyl[cyclohexyl(methoxymethoxy)methyl]stannane

Base Information

Chemical Name:Tributyl[cyclohexyl(methoxymethoxy)methyl]stannane
CAS No.:113248-99-0
Molecular Formula:C21H44O2Sn
Molecular Weight:447.289
Hs Code.:
DSSTox Substance ID:DTXSID40551485
Mol file:113248-99-0.mol

Synonyms:113248-99-0;TRIBUTYL[CYCLOHEXYL(METHOXYMETHOXY)METHYL]STANNANE;DTXSID40551485

Suppliers and Price of Tributyl[cyclohexyl(methoxymethoxy)methyl]stannane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Tributyl[cyclohexyl(methoxymethoxy)methyl]stannane

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:14
Exact Mass:448.236333
Heavy Atom Count:24
Complexity:268

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC[Sn](CCCC)(CCCC)C(C1CCCCC1)OCOC

Technology Process of Tributyl[cyclohexyl(methoxymethoxy)methyl]stannane

There total 2 articles about Tributyl[cyclohexyl(methoxymethoxy)methyl]stannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₄₀OSn

: 107-30-2
chloromethyl methyl ether

: 113248-99-0
tributyl(cyclohexyl(methoxymethoxy)methyl)stannane

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 0 - 23 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.jmedchem.6b01592

Reference yield:

: 688-73-3
tri-n-butyl-tin hydride

: 2043-61-0
cyclohexanecarbaldehyde

: 113248-99-0
tributyl(cyclohexyl(methoxymethoxy)methyl)stannane

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; hexane / 1 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 °C / Inert atmosphere

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 0 - 23 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/acs.jmedchem.6b01592

Reference yield: 72.0%

: 930-68-7
cyclohexenone

: 113248-99-0
tributyl(cyclohexyl(methoxymethoxy)methyl)stannane

: 113249-09-5
3-<(cyclohexyl)methoxymethoxymethyl>cyclohexanone

Guidance literature:: tributyl(cyclohexyl(methoxymethoxy)methyl)stannane; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.5h; Inert atmosphere;

With copper(l) cyanide; In tetrahydrofuran; hexane; at -30 ℃; for 1h; Inert atmosphere;

cyclohexenone; With chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acs.jmedchem.6b01592