2-Azido-5-methyl-3-nitrobenzaldehyde

Base Information

Chemical Name:2-Azido-5-methyl-3-nitrobenzaldehyde
CAS No.:113302-64-0
Molecular Formula:C8H6N4O3
Molecular Weight:206.161
Hs Code.:
DSSTox Substance ID:DTXSID00555606
Wikidata:Q82437002

Synonyms:2-Azido-5-methyl-3-nitrobenzaldehyde;113302-64-0;DTXSID00555606

Suppliers and Price of 2-Azido-5-methyl-3-nitrobenzaldehyde

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Azido-5-methyl-3-nitrobenzaldehyde

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:2
Exact Mass:206.04399007
Heavy Atom Count:15
Complexity:308

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)[N+](=O)[O-])N=[N+]=[N-])C=O

Technology Process of 2-Azido-5-methyl-3-nitrobenzaldehyde

There total 3 articles about 2-Azido-5-methyl-3-nitrobenzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113302-82-2
Toluene-4-sulfonate1-(2-formyl-4-methyl-6-nitro-phenyl)-pyridinium;

: 113302-64-0
2-azido-5-methyl-3-nitrobenzaldehyde

Guidance literature:: With sodium azide; In water; for 10h; Yield given; Ambient temperature;
DOI:10.1021/jo00244a038

Reference yield:

: 66620-31-3
2-hydroxy-5-methyl-3-nitro-benzaldehyde

: 113302-64-0
2-azido-5-methyl-3-nitrobenzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: 2 h / 90 °C

2: sodium azide / H₂O / 10 h / Ambient temperature

With sodium azide; In water;
DOI:10.1021/jo00244a038

Reference yield:

: 613-84-3
2-hydroxy-5-methylbenzaldehyde

: 113302-64-0
2-azido-5-methyl-3-nitrobenzaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 65 percent / fuming nitric acid / 0 °C

2: 2 h / 90 °C

3: sodium azide / H₂O / 10 h / Ambient temperature

With sodium azide; nitric acid; In water;
DOI:10.1021/jo00244a038