Technology Process of Benzene, [(3,3-dimethyl-2-phenylbutyl)thio]-
There total 5 articles about Benzene, [(3,3-dimethyl-2-phenylbutyl)thio]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
In
dimethyl sulfoxide;
Irradiation (UV/VIS); mercurial and organic compound dissolved in nitrogen purged solvent, irradn. (350-nm Rayonet photoreactor, 35-40°C, 24h); excess of NaBH4 added; stirred for 10-15 min; benzene added;; mixt. washed (H2O), dried (Na2SO4) and concd.;;
DOI:10.1021/ja00219a030
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dimethylsulfoxide / 12 h / 35 - 45 °C / Irradiation
2: dimethylsulfoxide / 24 h / 35 - 45 °C / Irradiation
3: 2.) NaBH4 / 1.) DMSO-d6, methylene dichloride, 35-40 deg C, 24 h.
With
sodium tetrahydroborate;
In
dimethyl sulfoxide;
DOI:10.1021/ja00219a030
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dimethylsulfoxide / 24 h / 35 - 45 °C / Irradiation
2: 2.) NaBH4 / 1.) DMSO-d6, methylene dichloride, 35-40 deg C, 24 h.
With
sodium tetrahydroborate;
In
dimethyl sulfoxide;
DOI:10.1021/ja00219a030
