2,2-diethoxy-N-phenylmethoxyethanamine

Base Information

Chemical Name:2,2-diethoxy-N-phenylmethoxyethanamine
CAS No.:113333-60-1
Molecular Formula:C13H21NO3
Molecular Weight:239.315
Hs Code.:
DSSTox Substance ID:DTXSID00553026

Synonyms:2,2-diethoxy-N-phenylmethoxyethanamine;113333-60-1;DTXSID00553026;AKOS019664189;2,2-diethoxy-ethyl-phenylmethoxy-amine;N-(Benzyloxy)-2,2-diethoxyethan-1-amine

Suppliers and Price of 2,2-diethoxy-N-phenylmethoxyethanamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,2-diethoxy-N-phenylmethoxyethanamine

Chemical Property:

XLogP3:1.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:9
Exact Mass:239.15214353
Heavy Atom Count:17
Complexity:166

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(CNOCC1=CC=CC=C1)OCC

Technology Process of 2,2-diethoxy-N-phenylmethoxyethanamine

There total 4 articles about 2,2-diethoxy-N-phenylmethoxyethanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 113333-55-4
Diethoxy-acetaldehyde O-benzyl-oxime

: 113333-60-1
1-Benzyloxyamino-2,2-diethoxyethane

Guidance literature:: With sodium cyanoborohydride; In ethanol; acetic acid; at 20 ℃; for 12h;
DOI:10.1055/s-1987-28029

Reference yield:

: 622-33-3
N-benzyloxyamine

: 2032-35-1
Bromoacetaldehyde diethyl acetal

: 113333-60-1
1-Benzyloxyamino-2,2-diethoxyethane

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; at 90 ℃; for 24h;
DOI:10.1021/jm9012592

Reference yield:

: 113333-49-6,113333-50-9
diethoxyacetaldehyde oxime

: 113333-60-1
1-Benzyloxyamino-2,2-diethoxyethane

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / C₂H₅ONa, KI / ethanol / 12 h / Heating

2: 77 percent / Na(BH₃CN) / acetic acid; ethanol / 12 h / 20 °C

With sodium ethanolate; sodium cyanoborohydride; potassium iodide; In ethanol; acetic acid;
DOI:10.1055/s-1987-28029