2-Butenoic acid, 4-oxo-4-phenyl-2-[(2,4,6-trimethylphenyl)amino]-, methyl ester

Base Information

Chemical Name:2-Butenoic acid, 4-oxo-4-phenyl-2-[(2,4,6-trimethylphenyl)amino]-, methyl ester
CAS No.:113416-27-6
Molecular Formula:C₂₀H₂₁NO₃
Molecular Weight:323.392
Hs Code.:
Mol file:113416-27-6.mol

Synonyms:(Z)-4-Oxo-4-phenyl-2-(2,4,6-trimethyl-phenylamino)-but-2-enoic acid methyl ester;

Suppliers and Price of 2-Butenoic acid, 4-oxo-4-phenyl-2-[(2,4,6-trimethylphenyl)amino]-, methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 2-Butenoic acid, 4-oxo-4-phenyl-2-[(2,4,6-trimethylphenyl)amino]-, methyl ester

Chemical Property:

PSA：55.40000
LogP:4.03650

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Butenoic acid, 4-oxo-4-phenyl-2-[(2,4,6-trimethylphenyl)amino]-, methyl ester

There total 3 articles about 2-Butenoic acid, 4-oxo-4-phenyl-2-[(2,4,6-trimethylphenyl)amino]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 41167-58-2
2-hydroxy-4-oxo-4-phenyl-but-2-enoic acid methyl ester

: 88-05-1
2,4,6-trimethylaniline

: 113416-27-6
Methyl-4-oxo-4-phenyl-2-(2,4,6-trimethylanilino)-2-butenoate

Guidance literature:: In benzene; for 12h; Heating;

Reference yield:

: 93-58-3,5705-52-2,80226-58-0
benzoic acid methyl ester

: 113416-27-6
Methyl-4-oxo-4-phenyl-2-(2,4,6-trimethylanilino)-2-butenoate

Guidance literature:: Multi-step reaction with 2 steps

1: BuLi / THF, HMPA, 30 min

2: 84 mg / diethyl ether

With n-butyllithium; In diethyl ether;
DOI:10.1246/bcsj.63.2408