Technology Process of But-2-enyltriethoxysilane
There total 1 articles about But-2-enyltriethoxysilane which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
trans-{Pt(tri-tert-butylphosphine)Cl}2; methylmagnesium chloride;
In
tetrahydrofuran; dichloromethane;
at -45 - 50 ℃;
Reagent/catalyst;
Solvent;
Overall yield = 85 %; Overall yield = 10.2 g;
Schlenk technique;
Sealed tube;
Inert atmosphere;
DOI:10.1021/ja5008596
- Guidance literature:
-
4-tolyl iodide; 2-butenyltriethoxysilane;
With
palladium(II) acetylacetonate; tetrabutyl ammonium fluoride; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene;
In
tetrahydrofuran;
Glovebox;
With
potassium pyrosulfite;
at 600 ℃;
Glovebox;
Inert atmosphere;
In
tetrahydrofuran;
at 20 - 80 ℃;
for 4h;
regioselective reaction;
Glovebox;
DOI:10.1039/c9cc06858a
