Ethanone, 1-[4-(4-methoxyphenyl)cyclohexyl]-, oxime, trans-

Base Information

Chemical Name:Ethanone, 1-[4-(4-methoxyphenyl)cyclohexyl]-, oxime, trans-
CAS No.:113524-47-3
Molecular Formula:C₁₅H₂₁NO₂
Molecular Weight:247.337
Hs Code.:

Synonyms:

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Chemical Property of Ethanone, 1-[4-(4-methoxyphenyl)cyclohexyl]-, oxime, trans-

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Technology Process of Ethanone, 1-[4-(4-methoxyphenyl)cyclohexyl]-, oxime, trans-

There total 4 articles about Ethanone, 1-[4-(4-methoxyphenyl)cyclohexyl]-, oxime, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21060-31-1
trans-1-(4-Phenylcyclohexyl)-1-ethanon

: 113524-47-3
ossima del trans-1-acetil-4-(4-metossifenil)cicloesano

Guidance literature:: Multi-step reaction with 5 steps

1: 72 percent / 90percent nitric acid / CHCl₃ / 1.5 h / -30 °C

2: 80 percent / hydrogen / 10percent Pd/C / ethyl acetate / Ambient temperature

3: 1.) 25percent sulfuric acid, sodium nitrite; 2.) conc. sulfuric acid / 1.) water, 0 deg C, 30 min; 2.) 1 h, r.t; 2 h, 70 deg C

4: 59 percent / 2percent sodium hydroxide / 7 h / Heating

5: 55 percent / hydroxylamine hydrochloride, sodium hydroxide / ethanol; H₂O / 7 h / Heating

With sodium hydroxide; sulfuric acid; hydroxylamine hydrochloride; hydrogen; nitric acid; sodium nitrite; palladium on activated charcoal; In ethanol; chloroform; water; ethyl acetate;

Reference yield:

: 113524-41-7
trans-1-acetil-4-(4-nitrofenil)cicloesano

: 113524-47-3
ossima del trans-1-acetil-4-(4-metossifenil)cicloesano

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / hydrogen / 10percent Pd/C / ethyl acetate / Ambient temperature

2: 1.) 25percent sulfuric acid, sodium nitrite; 2.) conc. sulfuric acid / 1.) water, 0 deg C, 30 min; 2.) 1 h, r.t; 2 h, 70 deg C

3: 59 percent / 2percent sodium hydroxide / 7 h / Heating

4: 55 percent / hydroxylamine hydrochloride, sodium hydroxide / ethanol; H₂O / 7 h / Heating

With sodium hydroxide; sulfuric acid; hydroxylamine hydrochloride; hydrogen; sodium nitrite; palladium on activated charcoal; In ethanol; water; ethyl acetate;

Reference yield:

: 113524-43-9
trans-1-acetil-4-(4-amminofenil)cicloesano

: 113524-47-3
ossima del trans-1-acetil-4-(4-metossifenil)cicloesano

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) 25percent sulfuric acid, sodium nitrite; 2.) conc. sulfuric acid / 1.) water, 0 deg C, 30 min; 2.) 1 h, r.t; 2 h, 70 deg C

2: 59 percent / 2percent sodium hydroxide / 7 h / Heating

3: 55 percent / hydroxylamine hydrochloride, sodium hydroxide / ethanol; H₂O / 7 h / Heating

With sodium hydroxide; sulfuric acid; hydroxylamine hydrochloride; sodium nitrite; In ethanol; water;