1-Methyl-2,5-diphenyl-4-[(trimethylsilyl)oxy]-1H-1,3-azaphosphole

Base Information

Chemical Name:1-Methyl-2,5-diphenyl-4-[(trimethylsilyl)oxy]-1H-1,3-azaphosphole
CAS No.:113545-93-0
Molecular Formula:C₁₉H₂₂NOPSi
Molecular Weight:339.449
Hs Code.:
DSSTox Substance ID:DTXSID80548713
Mol file:113545-93-0.mol

Synonyms:113545-93-0;DTXSID80548713;1-Methyl-2,5-diphenyl-4-[(trimethylsilyl)oxy]-1H-1,3-azaphosphole

Suppliers and Price of 1-Methyl-2,5-diphenyl-4-[(trimethylsilyl)oxy]-1H-1,3-azaphosphole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 1-Methyl-2,5-diphenyl-4-[(trimethylsilyl)oxy]-1H-1,3-azaphosphole

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:339.12082786
Heavy Atom Count:23
Complexity:374

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CN1C(=C(P=C1C2=CC=CC=C2)O[Si](C)(C)C)C3=CC=CC=C3

Technology Process of 1-Methyl-2,5-diphenyl-4-[(trimethylsilyl)oxy]-1H-1,3-azaphosphole

There total 1 articles about 1-Methyl-2,5-diphenyl-4-[(trimethylsilyl)oxy]-1H-1,3-azaphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 13712-75-9,165618-44-0
3-methyl-2,4-diphenyloxazolium-5-olate

: 15573-38-3
Tris(trimethylsilyl)phosphane

: 113545-93-0
1-Methyl-2,5-diphenyl-4-trimethylsilanyloxy-1H-[1,3]azaphosphole

Guidance literature:: In toluene; for 24h; Heating;
DOI:10.1016/S0040-4039(00)95918-5

Reference yield: 64.0%

: 113545-93-0
1-Methyl-2,5-diphenyl-4-trimethylsilanyloxy-1H-[1,3]azaphosphole

: 113545-96-3
1-Methyl-2,5-diphenyl-1H-[1,3]azaphosphol-4-ol

Guidance literature:: In methanol; Ambient temperature;
DOI:10.1016/S0040-4039(00)95918-5

Reference yield:

: 113545-93-0
1-Methyl-2,5-diphenyl-4-trimethylsilanyloxy-1H-[1,3]azaphosphole

: 113546-00-2
Benzoic acid 1-methyl-2,5-diphenyl-1H-[1,3]azaphosphol-4-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: KF, <18>-crown-6 / benzene / Ambient temperature

2: 40 percent

With potassium fluoride; 18-crown-6 ether; In benzene;
DOI:10.1016/S0040-4039(00)95918-5