Cyclopropanecarboxylic acid, 2,2-dimethyl-1-[(methylthio)(phenylimino)methyl]-3-[(trimethylsilyl)oxy]-, methyl ester

Base Information

Chemical Name:Cyclopropanecarboxylic acid, 2,2-dimethyl-1-[(methylthio)(phenylimino)methyl]-3-[(trimethylsilyl)oxy]-, methyl ester
CAS No.:113568-50-6
Molecular Formula:C₁₈H₂₇NO₃SSi
Molecular Weight:365.569
Hs Code.:
Mol file:113568-50-6.mol

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Chemical Property of Cyclopropanecarboxylic acid, 2,2-dimethyl-1-[(methylthio)(phenylimino)methyl]-3-[(trimethylsilyl)oxy]-, methyl ester

Chemical Property:

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Technology Process of Cyclopropanecarboxylic acid, 2,2-dimethyl-1-[(methylthio)(phenylimino)methyl]-3-[(trimethylsilyl)oxy]-, methyl ester

There total 1 articles about Cyclopropanecarboxylic acid, 2,2-dimethyl-1-[(methylthio)(phenylimino)methyl]-3-[(trimethylsilyl)oxy]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 77903-45-8
methyl 2,2-dimethyl-3-(trimethylsiloxy)-1-cyclopropanecarboxylate

: 103-72-0
phenyl isothiocyanate

: 74-88-4
methyl iodide

: 113568-50-6
3,3-Dimethyl-1--2-(trimethylsiloxy)cyclopropancarbonsauere-methylester

Guidance literature:: Yield given. Multistep reaction;

Reference yield: 29.0%

: 113568-50-6
3,3-Dimethyl-1--2-(trimethylsiloxy)cyclopropancarbonsauere-methylester

: 113568-41-5
4,5-Dihydro-5-hydroxy-2-(methylthio)-1-phenyl-1H-pyrrol-3-carbonsauere-methylester

Guidance literature:: With tetrabutyl ammonium fluoride; In dichloromethane;

Reference yield:

: 113568-50-6
3,3-Dimethyl-1--2-(trimethylsiloxy)cyclopropancarbonsauere-methylester

: 113568-47-1
4,5-Dihydro-4,4-dimethyl-2-(methylthio)-5-oxo-1-phenyl-1H-pyrrol-3-carbonsauere-methylester

Guidance literature:: Multi-step reaction with 2 steps

1: 29 percent / Bu₄NF / CH₂Cl₂

2: 48 percent / pyridiniumdichromate / CH₂Cl₂ / 168 h / Ambient temperature

With dipyridinium dichromate; tetrabutyl ammonium fluoride; In dichloromethane;