Technology Process of Benzoic acid, 2,6-bis[[3,5-bis(chlorocarbonyl)phenoxy]methyl]-, ethyl
ester
There total 8 articles about Benzoic acid, 2,6-bis[[3,5-bis(chlorocarbonyl)phenoxy]methyl]-, ethyl
ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
thionyl chloride;
In
N,N-dimethyl-formamide;
for 8h;
Heating;
DOI:10.1021/ja00219a023
- Guidance literature:
-
Multi-step reaction with 6 steps
1: thionyl chloride / dimethylformamide / 4 h / Ambient temperature
2: 8.7 g / Et3N / CH2Cl2 / 1 h
3: 23 percent / N-bromosuccinimide, benzoyl peroxide / CCl4 / 3 h / Heating
4: 95 percent / K2CO3 / dimethylformamide / 4 h
5: 95 percent / CF3CO2H / CH2Cl2 / 4 h / Ambient temperature
6: thionyl chloride / dimethylformamide / 8 h / Heating
With
N-Bromosuccinimide; thionyl chloride; Perbenzoic acid; potassium carbonate; triethylamine; trifluoroacetic acid;
In
tetrachloromethane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja00219a023
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 100 percent / acetone / 5 h / 0 °C
2: 95 percent / K2CO3 / dimethylformamide / 4 h
3: 95 percent / CF3CO2H / CH2Cl2 / 4 h / Ambient temperature
4: thionyl chloride / dimethylformamide / 8 h / Heating
With
thionyl chloride; potassium carbonate; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja00219a023