5-(aminosulfonyl)-2-methoxy-N-(1-methyl-4-piperidinyl)benzamide

Base Information

Chemical Name:5-(aminosulfonyl)-2-methoxy-N-(1-methyl-4-piperidinyl)benzamide
CAS No.:113681-64-4
Molecular Formula:C14H21N3O4S
Molecular Weight:327.39900
Hs Code.:
Mol file:113681-64-4.mol

Synonyms:2-Methoxy-N-(1-methyl-piperidin-4-yl)-5-sulfamoyl-benzamide;

Suppliers and Price of 5-(aminosulfonyl)-2-methoxy-N-(1-methyl-4-piperidinyl)benzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(aminosulfonyl)-2-methoxy-N-(1-methyl-4-piperidinyl)benzamide

Chemical Property:

PSA：110.11000
LogP:2.27650

Purity/Quality:

Safty Information:

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Technology Process of 5-(aminosulfonyl)-2-methoxy-N-(1-methyl-4-piperidinyl)benzamide

There total 2 articles about 5-(aminosulfonyl)-2-methoxy-N-(1-methyl-4-piperidinyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 41838-46-4
4-Amino-1-methylpiperidine

: 33045-53-3
2-methoxy-5-sulfamoylbenzoic acid ethyl ester

: 113681-64-4
N-(1-methyl-4-piperidinyl)-5-(aminosulfonyl)-2-methoxybenzamide

Guidance literature:: With sodium hydride; 1.) 100 deg C, 5 h; 2.) 120-130 deg C, 6 h;

Reference yield:

: 33045-52-2
methyl 2-methoxy-5-sulfamoyl-benzoate

: 113681-64-4
N-(1-methyl-4-piperidinyl)-5-(aminosulfonyl)-2-methoxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / H₂SO₄ / 12 h / Heating

2: 54 percent / NaH / 1.) 100 deg C, 5 h; 2.) 120-130 deg C, 6 h

With sulfuric acid; sodium hydride;