1(2H)-Pyridinecarboxylic acid, 4-[[[2-[[4-(methylamino)-1,2,5-thiadiazol-3-yl]amino]ethyl]thio]methyl]-, phenyl ester, S,S-dioxide

Base Information

Chemical Name:1(2H)-Pyridinecarboxylic acid, 4-[[[2-[[4-(methylamino)-1,2,5-thiadiazol-3-yl]amino]ethyl]thio]methyl]-, phenyl ester, S,S-dioxide
CAS No.:113697-79-3
Molecular Formula:C18H21N5O4S2
Molecular Weight:435.528
Hs Code.:
Mol file:113697-79-3.mol

Synonyms:

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Chemical Property of 1(2H)-Pyridinecarboxylic acid, 4-[[[2-[[4-(methylamino)-1,2,5-thiadiazol-3-yl]amino]ethyl]thio]methyl]-, phenyl ester, S,S-dioxide

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Technology Process of 1(2H)-Pyridinecarboxylic acid, 4-[[[2-[[4-(methylamino)-1,2,5-thiadiazol-3-yl]amino]ethyl]thio]methyl]-, phenyl ester, S,S-dioxide

There total 3 articles about 1(2H)-Pyridinecarboxylic acid, 4-[[[2-[[4-(methylamino)-1,2,5-thiadiazol-3-yl]amino]ethyl]thio]methyl]-, phenyl ester, S,S-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 113697-67-9
4-methylamino-3-<2-(4-pyridylmethylthio)ethylamino>-1,2,5-thiadiazole-1,1-dioxide

: 1885-14-9
phenyl chloroformate

: 113697-79-3
4-[2-(4-Methylamino-1,1-dioxo-1H-1λ⁶-[1,2,5]thiadiazol-3-ylamino)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

Guidance literature:: With sodium tetrahydroborate; In methanol; diethyl ether; at -65 ℃; for 5h;
DOI:10.1016/0223-5234(87)90269-8

Reference yield:

: 57667-43-3
4-<(2-aminoethyl)thiomethyl>pyridine

: 113697-79-3
4-[2-(4-Methylamino-1,1-dioxo-1H-1λ⁶-[1,2,5]thiadiazol-3-ylamino)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 1 h / 25 °C

2: methanol / 2 h / 25 °C

3: 57 percent / NaBH₄ / methanol; diethyl ether / 5 h / -65 °C

With sodium tetrahydroborate; In methanol; diethyl ether;
DOI:10.1016/0223-5234(87)90269-8

Reference yield:

: (4-Methoxy-1,1-dioxo-1H-1λ⁶-[1,2,5]thiadiazol-3-yl)-[2-(pyridin-4-ylmethylsulfanyl)-ethyl]-amine

: 113697-79-3
4-[2-(4-Methylamino-1,1-dioxo-1H-1λ⁶-[1,2,5]thiadiazol-3-ylamino)-ethylsulfanylmethyl]-2H-pyridine-1-carboxylic acid phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 2 h / 25 °C

2: 57 percent / NaBH₄ / methanol; diethyl ether / 5 h / -65 °C

With sodium tetrahydroborate; In methanol; diethyl ether;
DOI:10.1016/0223-5234(87)90269-8