Nirtetralin

Base Information

Chemical Name:Nirtetralin
CAS No.:78185-63-4
Molecular Formula:C₂₄H₃₀O₇
Molecular Weight:430.498
Hs Code.:
Mol file:78185-63-4.mol

Synonyms:Naphtho[2,3-d]-1,3-dioxole, 5-(3,4-dimethoxyphenyl)-5,6,7,8-tetrahydro-4-methoxy-6,7-bis(methoxymethyl)-, (5R,6S,7S)-rel-;rel-(5R,6S,7S)-5-(3,4-Dimethoxyphenyl)-5,6,7,8-tetrahydro-4-methoxy-6,7-bis(methoxymethyl)naphtho[2,3-d]-1,3-dioxole;Naphtho[2,3-d]-1,3-dioxole, 5-(3,4-dimethoxyphenyl)-5,6,7,8-tetrahydro-4-methoxy-6,7-bis(methoxymethyl)-, (5α,6β,7α)-(±)-;

Suppliers and Price of Nirtetralin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
Nirtetralin ≥98%
5mg
$ 468.00

Total 4 raw suppliers

Chemical Property of Nirtetralin

Chemical Property:

Vapor Pressure:4.43E-10mmHg at 25°C
Boiling Point:511.7°Cat760mmHg
Flash Point:201.1°C
PSA：64.61000
Density:1.158g/cm³
LogP:3.65430

Purity/Quality:

Analysis control,HPLC≥95% ^*data from raw suppliers

Nirtetralin ≥98% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Nirtetralin

There total 7 articles about Nirtetralin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5780-07-4
3-methoxy-4,5-methylenedioxybenzaldehyde

: 50656-78-5,78185-63-4
(+/-)-nirtetralin

Guidance literature:: Multi-step reaction with 7 steps

2: Pd-C

3: 2.) calcium borohydride

4: 1.) lithium di-isopropylamide

5: trifluoroacetic acid

6: lithium aluminium hydride

7: dimethylsulfoxide

With lithium aluminium tetrahydride; calcium borohydride; trifluoroacetic acid; lithium diisopropyl amide; palladium on activated charcoal; In dimethyl sulfoxide;
DOI:10.1016/0040-4039(81)80108-6

Reference yield:

: 78173-83-8
(E)-3-methoxycarbonyl-4-<5-methoxy-3,4-(methylenedioxy)phenyl>but-3-enoic acid

: 50656-78-5,78185-63-4
(+/-)-nirtetralin

Guidance literature:: Multi-step reaction with 6 steps

1: Pd-C

2: 2.) calcium borohydride

3: 1.) lithium di-isopropylamide

4: trifluoroacetic acid

5: lithium aluminium hydride

6: dimethylsulfoxide

With lithium aluminium tetrahydride; calcium borohydride; trifluoroacetic acid; lithium diisopropyl amide; palladium on activated charcoal; In dimethyl sulfoxide;
DOI:10.1016/0040-4039(81)80108-6

Reference yield:

: 78173-85-0,82467-46-7
trans-2-(α-hydroxy-3,4-dimethoxybenzyl)-3-(3-methoxy-4,5-methylenedioxybenzyl)butyrolactone

: 50656-78-5,78185-63-4
(+/-)-nirtetralin

Guidance literature:: Multi-step reaction with 3 steps

1: 320 mg / TFA / CH₂Cl₂ / 3 h / Ambient temperature

2: LiAlH₄ / tetrahydrofuran / 3 h / Ambient temperature

3: 129 mg / NaH / dimethylsulfoxide / 2.5 h / Ambient temperature

With lithium aluminium tetrahydride; sodium hydride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide;