D-Valine, N-[S-(diphenylmethyl)-L-cysteinyl]-, diphenylmethyl ester

Base Information

Chemical Name:D-Valine, N-[S-(diphenylmethyl)-L-cysteinyl]-, diphenylmethyl ester
CAS No.:113787-88-5
Molecular Formula:C34H36N2O3S
Molecular Weight:552.737
Hs Code.:
Mol file:113787-88-5.mol

Synonyms:

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Chemical Property of D-Valine, N-[S-(diphenylmethyl)-L-cysteinyl]-, diphenylmethyl ester

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Technology Process of D-Valine, N-[S-(diphenylmethyl)-L-cysteinyl]-, diphenylmethyl ester

There total 3 articles about D-Valine, N-[S-(diphenylmethyl)-L-cysteinyl]-, diphenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 113787-87-4
N-(t-butyloxycarbonyl)-S-(diphenylmethyl)-L-cysteinyl-D-valine benzhydryl ester

: 113787-88-5
S-(diphenylmethyl)-L-cysteinyl-D-valine benzhydryl ester

Guidance literature:: With toluene-4-sulfonic acid; In diethyl ether; ethanol; for 0.25h; Ambient temperature;
DOI:10.1016/S0040-4020(01)81664-1

Reference yield:

: 5191-80-0
S-diphenylmethyl-L-cysteine

: 113787-88-5
S-(diphenylmethyl)-L-cysteinyl-D-valine benzhydryl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 88 percent / 1M aqueous sodium hydroxide / H₂O; dioxane / Ambient temperature

2: 100 percent / EEDQ / CH₂Cl₂

3: 100 percent / p-toluenesulfonic acid / diethyl ether; ethanol / 0.25 h / Ambient temperature

With sodium hydroxide; toluene-4-sulfonic acid; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In 1,4-dioxane; diethyl ether; ethanol; dichloromethane; water;
DOI:10.1016/S0040-4020(01)81664-1

Reference yield:

: 21947-97-7
N-(t-butyloxycarbonyl)-S-(diphenylmethyl)-L-cysteine

: 113787-88-5
S-(diphenylmethyl)-L-cysteinyl-D-valine benzhydryl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / EEDQ / CH₂Cl₂

2: 100 percent / p-toluenesulfonic acid / diethyl ether; ethanol / 0.25 h / Ambient temperature

With toluene-4-sulfonic acid; N-ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)81664-1