2,4-Dioxa-7-aza-3-phosphaoctan-8-oic acid, 3-(4-chlorophenoxy)-1-(2,2-dimethyl-1,3-dioxolan-4-yl)-, 1,1-dimethylethyl ester, 3-oxide

Base Information

Chemical Name:2,4-Dioxa-7-aza-3-phosphaoctan-8-oic acid, 3-(4-chlorophenoxy)-1-(2,2-dimethyl-1,3-dioxolan-4-yl)-, 1,1-dimethylethyl ester, 3-oxide
CAS No.:113813-42-6
Molecular Formula:C19H29ClNO8P
Molecular Weight:465.868
Hs Code.:
Mol file:113813-42-6.mol

Synonyms:

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Chemical Property of 2,4-Dioxa-7-aza-3-phosphaoctan-8-oic acid, 3-(4-chlorophenoxy)-1-(2,2-dimethyl-1,3-dioxolan-4-yl)-, 1,1-dimethylethyl ester, 3-oxide

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Technology Process of 2,4-Dioxa-7-aza-3-phosphaoctan-8-oic acid, 3-(4-chlorophenoxy)-1-(2,2-dimethyl-1,3-dioxolan-4-yl)-, 1,1-dimethylethyl ester, 3-oxide

There total 3 articles about 2,4-Dioxa-7-aza-3-phosphaoctan-8-oic acid, 3-(4-chlorophenoxy)-1-(2,2-dimethyl-1,3-dioxolan-4-yl)-, 1,1-dimethylethyl ester, 3-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 26690-80-2
2-(N-tert-butoxycarbonylamino)ethanol

: 113813-41-5
(2-Oxo-oxazol-3-yl)-phosphonic acid 4-chloro-phenyl ester 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

: 113813-42-6
{2-[(4-Chloro-phenoxy)-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: zirconium acetylacetonate; In tetrahydrofuran; at 25 ℃;
DOI:10.1016/S0040-4039(00)96128-8

Reference yield:

: 100-79-8,36543-79-0
(R,S)-2,2-dimethyl-1,3-dioxolane-4-methanol

: 113813-42-6
{2-[(4-Chloro-phenoxy)-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / Mn(acac)3 / tetrahydrofuran / 25 °C

2: 54 percent / Zr(acac)4 / tetrahydrofuran / 25 °C

zirconium acetylacetonate; manganese(III) acetylacetonate; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)96128-8

Reference yield:

: 772-79-2
4-chlorophenylphosphorodichloridate

: 113813-42-6
{2-[(4-Chloro-phenoxy)-(2,2-dimethyl-[1,3]dioxolan-4-ylmethoxy)-phosphoryloxy]-ethyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 62 percent / Mn(acac)3 / tetrahydrofuran / 25 °C

2: 54 percent / Zr(acac)4 / tetrahydrofuran / 25 °C

zirconium acetylacetonate; manganese(III) acetylacetonate; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)96128-8