Dibenzo(a,g)quinolizinium, 5,6-dihydro-2,3,9,10-tetramethoxy-13-methyl-, iodide

Base Information

Chemical Name:Dibenzo(a,g)quinolizinium, 5,6-dihydro-2,3,9,10-tetramethoxy-13-methyl-, iodide
CAS No.:37553-95-0
Molecular Formula:C22H24INO4
Molecular Weight:493.3347
Hs Code.:
DSSTox Substance ID:DTXSID30958626

Synonyms:Dehydrocorydaline iodide;13-Methylpalmatine iodide;37553-95-0;Dibenzo(a,g)quinolizinium, 5,6-dihydro-2,3,9,10-tetramethoxy-13-methyl-, iodide;5,6-Dihydro-2,3,9,10-tetramethoxy-13-methyldibenzo(a,g)quinolizinium iodide;C22H24NO4.I;DTXSID30958626;C22-H24-N-O4.I;2,3,9,10-Tetramethoxy-13-methyl-5,6-dihydroisoquinolino[3,2-a]isoquinolin-7-ium iodide

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Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Dibenzo(a,g)quinolizinium, 5,6-dihydro-2,3,9,10-tetramethoxy-13-methyl-, iodide

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:g/cm³
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:4
Exact Mass:493.07501
Heavy Atom Count:28
Complexity:503

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C=CC(=C(C2=C[N+]3=C1C4=CC(=C(C=C4CC3)OC)OC)OC)OC.[I-]

Technology Process of Dibenzo(a,g)quinolizinium, 5,6-dihydro-2,3,9,10-tetramethoxy-13-methyl-, iodide

There total 10 articles about Dibenzo(a,g)quinolizinium, 5,6-dihydro-2,3,9,10-tetramethoxy-13-methyl-, iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 75875-59-1
dihydropalmatine chloride

: 37553-95-0
dehydrocorydaline

Guidance literature:: With sodium acetate; acetic acid; sodium iodide; for 0.25h; Heating;

Reference yield:

: 15248-39-2
6,7-dimethoxyisoquinoline

: 37553-95-0
dehydrocorydaline

Guidance literature:: Multi-step reaction with 5 steps

1: 86 percent / benzene / 24 h / Heating

2: 2.14 M n-BuLi / tetrahydrofuran; hexane / -35 °C

3: 383 mg / NaCNBH₃ / methanol; acetic acid / 0.25 h

4: 90 percent / conc. hydrochloric acud / Heating

5: 68 percent / 1.) 10 percent acetic acid, sodium acetate, 2.) NaI / 0.25 h / Heating

With hydrogenchloride; n-butyllithium; sodium acetate; sodium cyanoborohydride; acetic acid; sodium iodide; In tetrahydrofuran; methanol; hexane; acetic acid; benzene;

Reference yield:

: 3382-18-1
6,7-dimethoxy-3,4-dihydro-isoquinoline

: 37553-95-0
dehydrocorydaline

Guidance literature:: Multi-step reaction with 4 steps

1: 89 percent / benzene / 24 h / Ambient temperature

2: 98 percent / n-BuLi / tetrahydrofuran; hexane / 1.) -35 deg C, 30 min, 2.) -30 deg C, 3 h

3: 90 percent / conc. hydrochloric acud / Heating

4: 68 percent / 1.) 10 percent acetic acid, sodium acetate, 2.) NaI / 0.25 h / Heating

With hydrogenchloride; n-butyllithium; sodium acetate; acetic acid; sodium iodide; In tetrahydrofuran; hexane; benzene;