2-Methyl-3-[4-(trimethylsilyl)but-3-yn-1-yl]cyclohexan-1-one

Base Information

Chemical Name:2-Methyl-3-[4-(trimethylsilyl)but-3-yn-1-yl]cyclohexan-1-one
CAS No.:113893-25-7
Molecular Formula:C14H24OSi
Molecular Weight:236.42500
Hs Code.:
DSSTox Substance ID:DTXSID10554887
Mol file:113893-25-7.mol

Synonyms:113893-25-7;DTXSID10554887;2-Methyl-3-[4-(trimethylsilyl)but-3-yn-1-yl]cyclohexan-1-one

Suppliers and Price of 2-Methyl-3-[4-(trimethylsilyl)but-3-yn-1-yl]cyclohexan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-Methyl-3-[4-(trimethylsilyl)but-3-yn-1-yl]cyclohexan-1-one

Chemical Property:

PSA：17.07000
LogP:3.65270
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:236.159641919
Heavy Atom Count:16
Complexity:313

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C(CCCC1=O)CCC#C[Si](C)(C)C

Technology Process of 2-Methyl-3-[4-(trimethylsilyl)but-3-yn-1-yl]cyclohexan-1-one

There total 1 articles about 2-Methyl-3-[4-(trimethylsilyl)but-3-yn-1-yl]cyclohexan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1121-18-2
2-methyl-2-cyclohexen-1-one

: 113893-38-2
ω-trimethylsilylbutynylmagnesium chloride

: 113893-25-7
2-methyl-3-(4-(trimethylsilyl)but-3-yn-1-yl)cyclohexan-1-one

Guidance literature:: copper(l) iodide; In tetrahydrofuran;
DOI:10.1021/ja00218a060

Reference yield: 88.0%

: 113893-25-7
2-methyl-3-(4-(trimethylsilyl)but-3-yn-1-yl)cyclohexan-1-one

: C₁₁H₁₅ClO

Guidance literature:: With N-chloro-succinimide; tetrabutyl ammonium fluoride; silver nitrate; In acetonitrile; at 0 ℃; for 20h; Inert atmosphere; Schlenk technique; Darkness;
DOI:10.1002/anie.201610021