2,7-Bis(diphenylamino)-9H-fluoren-9-one

Base Information

Chemical Name:2,7-Bis(diphenylamino)-9H-fluoren-9-one
CAS No.:113933-91-8
Molecular Formula:C37H26N2O
Molecular Weight:514.626
Hs Code.:
DSSTox Substance ID:DTXSID50572843
Nikkaji Number:J1.258.582I
Wikidata:Q82461338
Mol file:113933-91-8.mol

Synonyms:113933-91-8;2,7-BIS(DIPHENYLAMINO)-9H-FLUOREN-9-ONE;SCHEMBL7740020;DTXSID50572843

Suppliers and Price of 2,7-Bis(diphenylamino)-9H-fluoren-9-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,7-Bis(diphenylamino)-9H-fluoren-9-one

Chemical Property:

XLogP3:9.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:6
Exact Mass:514.204513457
Heavy Atom Count:40
Complexity:716

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N(C2=CC=CC=C2)C3=CC4=C(C=C3)C5=C(C4=O)C=C(C=C5)N(C6=CC=CC=C6)C7=CC=CC=C7

Technology Process of 2,7-Bis(diphenylamino)-9H-fluoren-9-one

There total 5 articles about 2,7-Bis(diphenylamino)-9H-fluoren-9-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 155926-52-6
N,N,N',N'-tetraphenyl-9H-fluorene-2,7-diamine

: 113933-91-8
2,7-bis(diphenylamino)-9H-fluoren-9-one

Guidance literature:: With air; graphene-supported KOH composite; In N,N-dimethyl-formamide; at 20 ℃; for 16h;
DOI:10.1002/cplu.201300123

Reference yield: 90.2%

: 14348-75-5
2,7-dibromofluorene-9-one

: 122-39-4
diphenylamine

: 113933-91-8
2,7-bis(diphenylamino)-9H-fluoren-9-one

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; sodium t-butanolate; In toluene; at 110 ℃; for 24h; Inert atmosphere; Schlenk technique;

Reference yield:

: 16433-88-8
2,7-dibromo-9H-fluorene

: 122-39-4
diphenylamine

: 113933-91-8
2,7-bis(diphenylamino)-9H-fluoren-9-one

Guidance literature:: With oxygen; N-benzyl-trimethylammonium hydroxide; sodium t-butanolate; dichlorobis(tri-O-tolylphosphine)palladium; Yield given. Multistep reaction; 1) toluene, 100 deg C, 6 h, 2) pyridine, 1 h;
DOI:10.1007/PL00013499