Carbamic acid, (5-(3-(diethylamino)-1-oxopropyl)-10,11-dihydro-5H-dibenz(b,f)azepin-3-yl)-, ethyl ester

Base Information

Chemical Name:Carbamic acid, (5-(3-(diethylamino)-1-oxopropyl)-10,11-dihydro-5H-dibenz(b,f)azepin-3-yl)-, ethyl ester
CAS No.:83275-55-2
Molecular Formula:C₂₄H₃₁N₃O₃
Molecular Weight:409.528
Hs Code.:
DSSTox Substance ID:DTXSID40232242
Wikidata:Q83113276
ChEMBL ID:CHEMBL1411493

Synonyms:BRN 4827823;Carbamic acid, (5-(3-(diethylamino)-1-oxopropyl)-10,11-dihydro-5H-dibenz(b,f)azepin-3-yl)-, ethyl ester;CHEMBL1411493;83275-55-2;ChemDiv1_027251;Oprea1_085000;Oprea1_687096;CBDivE_008885;MLS001206511;SCHEMBL19224848;HMS664G15;DTXSID40232242;HMS2829N03;BDBM50146319;STK722314;AKOS000548818;NCGC00245321-01;SMR000517204;SR-01000597328;SR-01000597328-1;ethyl [5-(N,N-diethyl-beta-alanyl)-10,11-dihydro-5H-dibenzo[b,f]azepin-3-yl]carbamate;[5-(3-Diethylamino-propionyl)-10,11-dihydro-5H-dibenzo[b,f]azepin-3-yl]-carbamic acid ethyl ester;ETHYL N-{5-[3-(DIETHYLAMINO)PROPANOYL]-10,11-DIHYDRO-5H-DIBENZO[B,F]AZEPIN-3-YL}CARBAMATE

Suppliers and Price of Carbamic acid, (5-(3-(diethylamino)-1-oxopropyl)-10,11-dihydro-5H-dibenz(b,f)azepin-3-yl)-, ethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Carbamic acid, (5-(3-(diethylamino)-1-oxopropyl)-10,11-dihydro-5H-dibenz(b,f)azepin-3-yl)-, ethyl ester

Chemical Property:

Vapor Pressure:1.26E-12mmHg at 25°C
Boiling Point:561.3°Cat760mmHg
Flash Point:293.2°C
Density:1.163g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:8
Exact Mass:409.23654186
Heavy Atom Count:30
Complexity:566

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCN(CC)CCC(=O)N1C2=CC=CC=C2CCC3=C1C=C(C=C3)NC(=O)OCC

Technology Process of Carbamic acid, (5-(3-(diethylamino)-1-oxopropyl)-10,11-dihydro-5H-dibenz(b,f)azepin-3-yl)-, ethyl ester

There total 8 articles about Carbamic acid, (5-(3-(diethylamino)-1-oxopropyl)-10,11-dihydro-5H-dibenz(b,f)azepin-3-yl)-, ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.8%

: 6972-41-4
N,N-diethyl-β-alanine

: 78816-40-7
3-carbethoxyamino-10,11-dihydro-5H-dibenzazepine

: 83275-55-2
ethyl (5-(3-(N,N-diethylamino)propanoyl)-10,11-dihydro-5H-dibenzo[b,f]azepin-3-yl)carbamate

Guidance literature:: With 2,4,6-tripropyl-1,3,5,2,4,6-trioxatriphosphinane-2,4,6-trioxide; for 12h; Reflux; Inert atmosphere;
DOI:10.1016/j.ejmech.2015.12.018

Reference yield:

: 10464-35-4
3-amino-10,11-dihydro-5H-dibenzazepine

: 83275-55-2
ethyl (5-(3-(N,N-diethylamino)propanoyl)-10,11-dihydro-5H-dibenzo[b,f]azepin-3-yl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: Na₂CO₃ / acetone; H₂O / 1.5 h

2: toluene / 4 h / Heating

3: toluene / 4 h / 70 - 110.8 °C

With sodium carbonate; In water; acetone; toluene;